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*公司*RL-C-08-011-II取樣及檢測制度system of sampling and inspecting 1、取樣人:由質(zhì)檢科設(shè)一名專職取樣員Sampler: one full-time sampler who is established by quality control section2、取樣地點:分割車間Place: cutting room3、取樣數(shù)量:每個樣品不少于1200GQuantity: each sample not less than 1200g4、 取樣方法:Sampling methods41專職取樣員在分割車間每舍雞割取胸肉樣約1200G,其中200G入樣品袋送化驗室檢測藥殘,其余1000G封存?zhèn)錂z,與前后兩舍雞相鄰的雞不取樣,每車雞要從不少于50-100只雞體上取樣。 The full-time sampler take samples of chicken breast about 1200g from every farmhouse.200g samples is sealed and sent to the lab for inspection of medicine residue, the others will be sealed up for keeping. The number of samples from each vehicle is not less than 50-100 birds42每個樣品均用標簽標明宰殺日期班次和場舍號,每2-3個樣品送化驗室一次,入冰箱內(nèi)保存,以備檢測。 Each sample should be marked the shift code and farmhouse code and slaughter date. Every 2-3 samples will be sent to the lab to seal up for keeping in the refrigerator one time.1、 化驗室樣品登記 Registration of samples51化驗室根據(jù)送樣單對樣品進行核對,對每舍雞進行編號登記,做好樣品登記表。 Each farmhouse is registered and made records in the lab according to the sampling list.2、 樣品檢測Inspection of sample61化驗室在接到樣品3小時內(nèi)進行前處理,按編號進行檢測。The sample is prepared and inspected within 3 hours after receiving according to the serial number 62化驗室根據(jù)操作規(guī)程將每家樣品進行檢測,根據(jù)檢測結(jié)果,出具藥殘檢測報告通知主檢獸醫(yī)和養(yǎng)殖公司,由主檢獸醫(yī)通知質(zhì)檢科及生產(chǎn)車間。The samples are inspected according to the operation regulation and the report of inspection will be informed to the chief veterinarians and the breeding company. Then the chief veterinarian will inform the result to the quality control section and the working shop.3、 不合格品處理Disposal of the unqualified products 71對于藥殘陽性的養(yǎng)雞場,由化驗室通知主檢獸醫(yī)、品保部及質(zhì)檢科,由生產(chǎn)車間根據(jù)相應(yīng)標識及時將該場雞的產(chǎn)品挑出隔離,質(zhì)檢科做好相應(yīng)的不合格品監(jiān)督處理記錄;同時化驗室通知養(yǎng)殖公司,對養(yǎng)殖場調(diào)查原因并做出相應(yīng)處理。The products which indicated positive result will be picked out and quarantined according to the related label in time in the workshop. Meanwhile the supervision and disposal records of unqualified products will be made by the quality control section. 4、 檢測儀器及方法instrument and method of inspection檢測項目 所用儀器 檢測依據(jù)inspection items instrument criterion of inspection克球酚 HPGC5890 SN0283-93clopidol HPGC5890 SN0283-93磺胺類 HPLC1100 日法sulfanilamide HPLC1100 Japanese method氯霉素 HPGC5890 SN0341-95cholramphenicol HPGC5890 SN0341-955、 報告記錄的管理management of record91檢測報告需填寫清晰、正確、完整,需經(jīng)檢測人及主管簽名并加蓋檢測專用章后方有效。Only the inspection report which is clear, correct ,complete and signed and stamped by the inspector and director is valid92實驗對檢測的原始記錄及相應(yīng)圖譜及檢測報告復(fù)寫件應(yīng)保存完好,每月裝訂一次入資料室存檔,所有記錄保存期為2年。The original and copy of inspection record , Chart should be completely kept. All records are binded every month and archived for 2 years.10、樣品的保存Preservation of the samples化驗室對每舍雞的檢測剩余樣做好標識,裝袋入冷藏庫保存,做好相應(yīng)的樣品入庫登記,所有樣品均保存三個月,以備查。The residu

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