贛榆海州灣生物科技園產(chǎn)業(yè)發(fā)展規(guī)劃環(huán)境影響評(píng)價(jià)環(huán)境現(xiàn)狀監(jiān)測(cè)檢測(cè)報(bào)告

檢測(cè)報(bào)告TESTREPORT編號(hào)：連智檢（2021）第164號(hào)項(xiàng)目名稱：

贛榆海州灣生物科技園產(chǎn)業(yè)發(fā)展規(guī)劃環(huán)境影響評(píng)價(jià)環(huán)境現(xiàn)狀監(jiān)測(cè)委托單位： 江蘇智盛環(huán)境科技有限公司檢測(cè)類別： 委托檢測(cè)報(bào)告日期： 2021年05月28日學(xué)院科技南樓層連云港智清環(huán)境科技有限公司 地址連云港市海州區(qū)晨光路2號(hào)連云港職業(yè)技學(xué)院科技南樓層4

電話測(cè)報(bào)告說明一、本報(bào)告無檢測(cè)檢驗(yàn)專用章、騎縫章、無審核簽發(fā)者簽字無效。二、對(duì)檢測(cè)結(jié)果如有異議者，請(qǐng)于收到報(bào)告之日起十日內(nèi)向連云港智清環(huán)境科技有限公司提出。逾期不提出，視為認(rèn)可檢測(cè)報(bào)告。三、本報(bào)告部分復(fù)制、私自冒用、涂改或以其它任何形式篡改均屬無效。經(jīng)同意復(fù)制的復(fù)制件，應(yīng)由連云港智清環(huán)境科技有限公司加蓋公章確認(rèn)。四、委托單位對(duì)樣品的代表性和真實(shí)性負(fù)責(zé)，檢測(cè)報(bào)告只對(duì)所檢樣品檢測(cè)項(xiàng)目的檢測(cè)結(jié)果負(fù)責(zé)，委托檢測(cè)結(jié)果及其對(duì)結(jié)果的判定結(jié)論只代表檢測(cè)時(shí)污染物排放狀況，排放標(biāo)準(zhǔn)由客戶提供。五、由委托單位自行采集的樣品，本檢驗(yàn)部門僅對(duì)送檢樣品檢驗(yàn)數(shù)據(jù)負(fù)責(zé)，不對(duì)樣品來源負(fù)責(zé)。六、除客戶特別申明并支付樣品管理費(fèi)，所有超過標(biāo)準(zhǔn)規(guī)定時(shí)效期的樣品均不再做留樣。七、本單位保證工作的客觀公正性，對(duì)委托單位的商業(yè)信息、技術(shù)文件等商業(yè)秘密履行保密義務(wù)?！?”檢測(cè)項(xiàng)目帶“☆”的，為本實(shí)驗(yàn)室無相應(yīng)資質(zhì)認(rèn)定許可技術(shù)能力分包項(xiàng)目。單位名稱：連云港智清環(huán)境科技有限公司聯(lián)系地址：連云港海州區(qū)晨光路2號(hào)連云港職業(yè)技術(shù)學(xué)院科技南樓4層聯(lián)系電話政編碼：222000連云港智清環(huán)境科技有限公司 連智檢（2021）第164號(hào)檢測(cè)報(bào)告委托單位江蘇智盛環(huán)境科技有限公司受檢單位/受檢單位地址/聯(lián)系人孫萬釗聯(lián)系電樣日期2021.05.06~05.12、05.21、05.23分析日期樣品來源采樣任務(wù)流轉(zhuǎn)卡號(hào)JC21153采樣人員樣品類別地表水、地下水、海水、環(huán)境空氣、噪聲、土壤、底泥、包氣帶檢測(cè)目的贛榆海州灣生物科技園產(chǎn)業(yè)發(fā)展規(guī)劃環(huán)境影響評(píng)價(jià)環(huán)境現(xiàn)狀監(jiān)測(cè)檢測(cè)內(nèi)容海 水化學(xué)需氧量氨氮硝酸鹽氮亞硝酸鹽氮活性磷酸鹽六價(jià)鉻石油類、鉛☆、鉻、銅☆、鋅☆、鎳☆地下水：pH值、鉀、鈉、鈣、鎂、碳酸根、重碳酸根、氯化物、硫酸鹽、氨氮、硝環(huán)境空氣：氨、硫化氫、臭氣濃度、氯化氫、氟化物、鉛、苯乙烯、甲苯、間二甲苯、對(duì)二甲苯、鄰二甲苯、硫酸霧、甲醇、乙醇、非甲烷總烴土 壤值汞砷銅鉛鎳鎘六價(jià)鉻氧化還原電位陽(yáng)離子交換量、容重、揮發(fā)性有機(jī)物、半揮發(fā)性有機(jī)物底 泥：銅、鋅、鎳、鉻、鎘、鉛、汞、砷噪 聲：等效連續(xù)A聲級(jí)檢測(cè)依據(jù)詳見第19~24頁(yè)檢測(cè)結(jié)果詳見第2~13頁(yè)備注1、ND為未檢出；2、檢測(cè)項(xiàng)目中帶“”項(xiàng)目分包蘇州環(huán)優(yōu)檢測(cè)有限公司，報(bào)告編號(hào)HY210556、HY210511057、HY210524023(CMA171012050352）。編制： 審核： 簽發(fā)： 簽發(fā)日期檢測(cè)機(jī)構(gòu)檢驗(yàn)章年 月日第1頁(yè)共27頁(yè)連智檢（2021）第連智檢（2021）第164號(hào)連云港智清環(huán)境科技有限公司第第16頁(yè)共27頁(yè)表（1）地表水檢測(cè)結(jié)果采樣地點(diǎn)采樣日期采樣時(shí)間檢測(cè)項(xiàng)目化學(xué)需氧量氟化物氨氮總磷石油類鉛六價(jià)鉻鋅mg/Lmg/Lmg/Lmg/Lmg/Lμg/Lmg/Lmg/L1#興莊河閘2021.05.1009:31260.581.040.230.0320.3ND0.0215:30280.611.390.260.0432.9ND0.023#官莊河老204國(guó)道交匯處10:02380.771.360.280.0337.8ND0.0616:01340.781.680.290.0443.1ND0.054#官莊河閘10:28330.721.440.320.0545.9ND0.0616:26370.721.720.330.0447.6ND0.08采樣地點(diǎn)采樣日期采樣時(shí)間銅甲苯間二甲苯對(duì)二甲苯鄰二甲苯苯乙烯鎳☆樣品性狀μg/Lμg/Lμg/Lμg/Lμg/Lμg/Lmg/L/1#興莊河閘2021.05.1009:3114.3NDNDNDNDND2.10×10-3淡黃微濁、微弱15:3017.7NDNDNDNDND2.28×10-3淡黃微濁、微弱3#官莊河老204國(guó)道交匯處10:0248.4NDNDNDNDND5.09×10-3淡黃微濁、微弱16:0146.9NDNDNDNDND5.37×10-3淡黃微濁、微弱4#官莊河閘10:2885.9NDNDNDNDND5.22×10-3淡黃微濁、微弱16:2695.2NDNDNDNDND0.0113淡黃微濁、微弱表（1）地表水檢測(cè)結(jié)果（續(xù)）采樣地點(diǎn)采樣日期采樣時(shí)間檢測(cè)項(xiàng)目化學(xué)需氧量氟化物氨氮總磷石油類鉛六價(jià)鉻鋅mg/Lmg/Lmg/Lmg/Lmg/Lμg/Lmg/Lmg/L1#興莊河閘2021.05.1109:30240.561.180.300.0421.3ND0.0215:27250.581.130.290.0520.3ND0.043#官莊河老204國(guó)道交匯處10:00300.711.400.270.0635.6ND0.0716:00400.741.440.250.0534.1ND0.074#官莊河閘10:27360.631.410.340.0748.6ND0.0916:27340.641.460.330.0648.6ND0.10采樣地點(diǎn)采樣日期采樣時(shí)間銅甲苯間二甲苯對(duì)二甲苯鄰二甲苯苯乙烯鎳☆樣品性狀μg/Lμg/Lμg/Lμg/Lμg/Lμg/Lmg/L/1#興莊河閘2021.05.1109:3019.0NDNDNDNDND3.77×10-3淡黃微濁、微弱15:2719.3NDNDNDNDND3.62×10-3淡黃微濁、微弱3#官莊河老204國(guó)道交匯處10:0045.6NDNDNDNDND0.0141淡黃微濁、微弱16:0045.1NDNDNDNDND0.0123淡黃微濁、微弱4#官莊河閘10:2778.1NDNDNDNDND0.0127淡黃微濁、微弱16:2796.6NDNDNDNDND0.0109淡黃微濁、微弱表（1）地表水檢測(cè)結(jié)果（續(xù)）采樣地點(diǎn)采樣日期采樣時(shí)間檢測(cè)項(xiàng)目化學(xué)需氧量氟化物氨氮總磷石油類鉛六價(jià)鉻鋅mg/Lmg/Lmg/Lmg/Lmg/Lμg/Lmg/Lmg/L1#興莊河閘2021.05.1209:33290.551.190.250.0419.3ND0.0215:26270.621.210.270.0433.6ND0.043#官莊河老204國(guó)道交匯處10:06350.761.480.330.0434.1ND0.0815:59340.751.480.310.0541.4ND0.084#官莊河閘10:32360.671.580.280.0642.6ND0.0916:25350.611.560.290.0646.6ND0.09采樣地點(diǎn)采樣日期采樣時(shí)間銅甲苯間二甲苯對(duì)二甲苯鄰二甲苯苯乙烯鎳☆樣品性狀μg/Lμg/Lμg/Lμg/Lμg/Lμg/Lmg/L/1#興莊河閘2021.05.1209:3312.4NDNDNDNDND2.48×10-3淡黃微濁、微弱15:2619.5NDNDNDNDND2.80×10-3淡黃微濁、微弱3#官莊河老204國(guó)道交匯處10:0647.2NDNDNDNDND5.31×10-3淡黃微濁、微弱15:5944.8NDNDNDNDND5.95×10-3淡黃微濁、微弱4#官莊河閘10:3278.1NDNDNDNDND0.0135淡黃微濁、微弱16:2597.4NDNDNDNDND0.0129淡黃微濁、微弱表（2）海水檢測(cè)結(jié)果采樣地點(diǎn)采樣日期采樣時(shí)間檢測(cè)項(xiàng)目化學(xué)需氧量氨硝酸鹽亞硝酸鹽活性磷酸鹽六價(jià)鉻石油類mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L2#老興莊河閘下(G228國(guó)道附近)2021.05.0709:102.660.1700.2150.02070.0246ND0.0515:112.340.1530.1310.01530.0235ND0.026#興莊河閘下近岸海域09:263.950.2180.2840.05900.0333ND0.1415:313.890.2050.2140.03050.0224ND0.035#沙旺河閘下近岸海域09:542.650.2210.2110.09050.0273ND0.0515:552.340.2100.1570.04080.0262ND0.03采樣地點(diǎn)采樣日期采樣時(shí)間鎳☆鉛☆銅☆鋅☆鉻☆//mg/Lmg/Lmg/Lmg/Lmg/L//2#老興莊河閘下(G228國(guó)道附近)2021.05.0709:104.5×10-32.23×10-30.01240.02937×10-4//15:114.2×10-32.49×10-30.01250.01063.8×10-3//6#興莊河閘下近岸海域09:264.3×10-34.79×10-30.01220.00853.6×10-3//15:314.2×10-32.09×10-30.01240.00962.8×10-3//5#沙旺河閘下近岸海域09:543.2×10-31.46×10-38.6×10-30.00963.6×10-3//15:554.3×10-32.11×10-30.01270.01062.8×10-3//表（2）海水檢測(cè)結(jié)果（續(xù)）采樣地點(diǎn)采樣日期采樣時(shí)間檢測(cè)項(xiàng)目化學(xué)需氧量氨硝酸鹽亞硝酸鹽活性磷酸鹽六價(jià)鉻石油類mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L2#老興莊河閘下(G228國(guó)道附近)2021.05.0809:362.680.1670.3100.02110.0197ND0.0415:362.220.1620.1730.01540.0191ND0.026#興莊河閘下近岸海域09:593.980.2140.2700.05930.0341ND0.1016:013.960.2350.2050.03080.0338ND0.035#沙旺河閘下近岸海域10:272.940.2180.2350.08900.0278ND0.0516:292.380.2000.2140.04050.0265ND0.03采樣地點(diǎn)采樣日期采樣時(shí)間鎳☆鉛☆銅☆鋅☆鉻☆//mg/Lmg/Lmg/Lmg/Lmg/L//2#老興莊河閘下(G228國(guó)道附近)2021.05.0809:363.0×10-31.39×10-33.2×10-30.02984×10-4//15:363.3×10-31.90×10-33.7×10-30.01705×10-4//6#興莊河閘下近岸海域09:593.5×10-31.98×10-33.5×10-30.02985×10-4//16:013.2×10-31.97×10-33.7×10-30.01491.8×10-3//5#沙旺河閘下近岸海域10:275.4×10-31.39×10-33.9×10-30.01542.7×10-3//16:295.1×10-31.90×10-33.6×10-3ND2.6×10-3//表（2）海水檢測(cè)結(jié)果（續(xù)）采樣地點(diǎn)采樣日期采樣時(shí)間檢測(cè)項(xiàng)目化學(xué)需氧量氨硝酸鹽亞硝酸鹽活性磷酸鹽六價(jià)鉻石油類mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L2#老興莊河閘下(G228國(guó)道附近)2021.05.0909:422.610.1680.3180.02100.0240ND0.0415:472.170.1620.1780.01530.0221ND0.036#興莊河閘下近岸海域10:113.980.2180.2360.06000.0300ND0.0916:203.950.2070.2140.03080.0276ND0.035#沙旺河閘下近岸海域10:342.810.2210.1940.08880.0267ND0.0516:492.400.2020.1610.04180.0254ND0.02采樣地點(diǎn)采樣日期采樣時(shí)間鎳☆鉛☆銅☆鋅☆鉻☆//mg/Lmg/Lmg/Lmg/Lmg/L//2#老興莊河閘下(G228國(guó)道附近)2021.05.0909:429.5×10-31.29×10-33.6×10-30.01177.0×10-4//15:473.1×10-31.19×10-33.1×10-30.02025.0×10-4//6#興莊河閘下近岸海域10:112.9×10-31.14×10-35.7×10-30.00962.7×10-3//16:203.3×10-31.89×10-33.6×10-30.01121.8×10-3//5#沙旺河閘下近岸海域10:343.3×10-39.9×10-40.01190.00962.7×10-3//16:495.6×10-37.15×10-37.1×10-30.02342.7×10-3//表（3）地下水檢測(cè)結(jié)果表采樣地點(diǎn)采樣日期采樣時(shí)間檢測(cè)項(xiàng)目pH值鉀鈉鈣鎂碳酸根重碳酸根氯化物硫酸根無量綱mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/LD12021.05.1216:566.7722.727015431.2ND39051881.2D217:248.5573.32.38×10341898.0562784.21×103618D317:497.862836.96×103827374ND4391.20×1042.09×103D418:167.2725.530118926.9ND430568179D518:507.282567.85×103863355ND4301.35×1042.06×103采樣地點(diǎn)采樣日期采樣時(shí)間檢測(cè)項(xiàng)目耗氧量（CODMn）總硬度（以CaCO3計(jì)）溶解性總固體硝酸鹽氮（以N計(jì)）亞硝酸鹽氮（N計(jì)）氨氮六價(jià)鉻銅鉛mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lμg/Lμg/LD12021.05.1216:560.826201.95×1031.2ND0.626ND15.421.4D217:2430.61.87×1039.20×1032.11.355.84ND49.436.3D317:493.324.55×1034.60×1040.50.0054.89ND90.962.1D418:164.537101.83×1030.20.0320.679ND17.714.9D518:504.295.25×1034.82×1040.60.0183.15ND80.964.4表（3）地下水檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣日期采樣時(shí)間檢測(cè)項(xiàng)目地下水檢測(cè)點(diǎn)位參數(shù)及樣品性狀統(tǒng)計(jì)表鋅甲苯對(duì)二甲苯間二甲苯鄰二甲苯鎳☆經(jīng)度緯度樣品性狀mg/Lμg/Lμg/Lμg/Lμg/Lmg/L///D12021.05.1216:560.07NDNDNDND8.30×10-4119.150759967034.9188860198無色透明、無味D217:240.04NDNDNDND0.0177119.179683170234.9197617750淡黃微濁、弱D317:490.10NDNDNDND5.13×10-3119.182922623234.9074296283淡黃微濁、微弱D418:160.13NDNDNDND3.59×10-3119.168746765734.8982262282淡黃微濁、微弱D518:500.26NDNDNDND8.54×10-3119.193072930234.9094913567淡黃微濁、微弱以下空白第第19頁(yè)共27頁(yè)表（4）環(huán)境空氣檢測(cè)結(jié)果表采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目氨mg/m3硫化氫mg/m3臭氣濃度無量綱氯化氫mg/m3氟化物μg/m3硫酸霧mg/m3非甲烷總烴mg/m3苯乙烯mg/m3甲苯mg/m3間二甲苯mg/m3G1匡口村（園區(qū)內(nèi)）2021.05.0602:000.050.003ND0.032ND0.0890.59NDNDND08:000.060.003ND0.027ND0.0880.62NDNDND14:000.080.005ND0.030ND0.0770.61NDNDND20:000.050.006ND0.029ND0.0750.62NDNDNDG2興莊村02:000.060.004ND0.041ND0.0910.49NDNDND08:000.060.003ND0.041ND0.0670.49NDNDND14:000.080.004ND0.032ND0.0830.53NDNDND20:000.060.006ND0.033ND0.0820.63NDNDNDG3李巷村02:000.060.003ND0.020ND0.0810.50NDNDND08:000.040.004ND0.018ND0.0960.43NDNDND14:000.040.005ND0.031ND0.0760.49NDNDND20:000.050.005ND0.017ND0.0800.47NDNDND表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目氨mg/m3硫化氫mg/m3臭氣濃度無量綱氯化氫mg/m3氟化物μg/m3硫酸霧mg/m3非甲烷總烴mg/m3苯乙烯mg/m3甲苯mg/m3間二甲苯mg/m3G1匡口村（園區(qū)內(nèi)）2021.05.0702:000.050.003ND0.036ND0.0900.52NDNDND08:000.070.003ND0.037ND0.0870.49NDNDND14:000.060.004ND0.029ND0.0790.48NDNDND20:000.040.005ND0.027ND0.0750.48NDNDNDG2興莊村02:000.030.006ND0.028ND0.0920.43NDNDND08:000.020.004ND0.026ND0.0680.43NDNDND14:000.070.006ND0.029ND0.0820.39NDNDND20:000.070.005ND0.032ND0.0820.46NDNDNDG3李巷村02:000.050.006ND0.029ND0.0790.58NDNDND08:000.050.004ND0.029ND0.1020.53NDNDND14:000.040.006ND0.029ND0.0770.59NDNDND20:000.030.003ND0.039ND0.0800.55NDNDND表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目氨mg/m3硫化氫mg/m3臭氣濃度無量綱氯化氫mg/m3氟化物μg/m3硫酸霧mg/m3非甲烷總烴mg/m3苯乙烯mg/m3甲苯mg/m3間二甲苯mg/m3G1匡口村（園區(qū)內(nèi)）2021.05.0802:000.050.003ND0.030ND0.0100.51NDNDND08:000.070.004ND0.033ND0.0110.35NDNDND14:000.030.005ND0.034ND0.0080.48NDNDND20:000.080.006ND0.032ND0.0080.50NDNDNDG2興莊村02:000.060.006ND0.032ND0.0100.74NDNDND08:000.060.004ND0.032ND0.0070.56NDNDND14:000.060.006ND0.032ND0.0090.63NDNDND20:000.060.004ND0.033ND0.0090.48NDNDNDG3李巷村02:000.060.003ND0.030ND0.0080.62NDNDND08:000.040.004ND0.034ND0.0100.50NDNDND14:000.070.003ND0.041ND0.0080.50NDNDND20:000.040.003ND0.040ND0.0080.56NDNDND表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目氨mg/m3硫化氫mg/m3臭氣濃度無量綱氯化氫mg/m3氟化物μg/m3硫酸霧mg/m3非甲烷總烴mg/m3苯乙烯mg/m3甲苯mg/m3間二甲苯mg/m3G1匡口村（園區(qū)內(nèi)）2021.05.0902:000.070.005ND0.020ND0.0100.47NDNDND08:000.060.003ND0.022ND0.0100.44NDNDND14:000.050.003ND0.016ND0.0080.45NDNDND20:000.030.004ND0.024ND0.0080.47NDNDNDG2興莊村02:000.060.004ND0.020ND0.0100.66NDNDND08:000.070.003ND0.022ND0.0070.66NDNDND14:000.040.004ND0.023ND0.0090.66NDNDND20:000.040.004ND0.043ND0.0090.66NDNDNDG3李巷村02:000.110.005ND0.040ND0.0080.42NDNDND08:000.040.005ND0.041ND0.0100.41NDNDND14:000.070.005ND0.019ND0.0070.47NDNDND20:000.060.006ND0.013ND0.0080.43NDNDND表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目氨mg/m3硫化氫mg/m3臭氣濃度無量綱氯化氫mg/m3氟化物μg/m3硫酸霧mg/m3非甲烷總烴mg/m3苯乙烯mg/m3甲苯mg/m3間二甲苯mg/m3G1匡口村（園區(qū)內(nèi)）2021.05.1002:000.050.004ND0.038ND0.0100.29NDNDND08:000.060.004ND0.038ND0.0100.25NDNDND14:000.070.006ND0.033ND0.0080.25NDNDND20:000.030.006ND0.023ND0.0080.27NDNDNDG2興莊村02:000.050.004ND0.023ND0.0100.34NDNDND08:000.050.006ND0.023ND0.0070.34NDNDND14:000.060.004ND0.041ND0.0090.31NDNDND20:000.090.002ND0.041ND0.0090.33NDNDNDG3李巷村02:000.040.004ND0.042ND0.0080.50NDNDND08:000.030.002ND0.029ND0.0100.44NDNDND14:000.050.004ND0.020ND0.0070.41NDNDND20:000.070.005ND0.019ND0.0080.37NDNDND表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目氨mg/m3硫化氫mg/m3臭氣濃度無量綱氯化氫mg/m3氟化物μg/m3硫酸霧mg/m3非甲烷總烴mg/m3苯乙烯mg/m3甲苯mg/m3間二甲苯mg/m3G1匡口村（園區(qū)內(nèi)）2021.05.1102:000.060.005ND0.020ND0.0100.30NDNDND08:000.050.003ND0.019ND0.0100.30NDNDND14:000.030.004ND0.019ND0.0090.31NDNDND20:000.060.005ND0.021ND0.0050.28NDNDNDG2興莊村02:000.060.004ND0.021ND0.0090.34NDNDND08:000.050.006ND0.020ND0.0090.39NDNDND14:000.050.005ND0.030ND0.0070.35NDNDND20:000.030.004ND0.028ND0.0090.34NDNDNDG3李巷村02:000.050.005ND0.027ND0.0070.40NDNDND08:000.060.005ND0.041ND0.0100.39NDNDND14:000.040.006ND0.042ND0.0090.35NDNDND20:000.050.006ND0.041ND0.0090.38NDNDND表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目氨mg/m3硫化氫mg/m3臭氣濃度無量綱氯化氫mg/m3氟化物μg/m3硫酸霧mg/m3非甲烷總烴mg/m3苯乙烯mg/m3甲苯mg/m3間二甲苯mg/m3G1匡口村（園區(qū)內(nèi)）2021.05.1202:000.050.005ND0.020ND0.0100.30NDNDND08:000.030.002ND0.019ND0.0100.28NDNDND14:000.050.004ND0.021ND0.0090.30NDNDND20:000.060.003ND0.021ND0.0070.32NDNDNDG2興莊村02:000.040.003ND0.021ND0.0090.45NDNDND08:000.060.004ND0.022ND0.0090.46NDNDND14:000.060.004NDNDND0.0080.46NDNDND20:000.080.003ND0.020ND0.0090.44NDNDNDG3李巷村02:000.060.004ND0.019ND0.0070.39NDNDND08:000.050.005ND0.019ND0.0090.37NDNDND14:000.090.005ND0.020ND0.0100.43NDNDND20:000.090.005ND0.019ND0.0090.40NDNDND表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目對(duì)二甲苯mg/m3鄰二甲苯mg/m3甲醇mg/m3乙醇mg/m3氣溫℃氣壓kPa風(fēng)向風(fēng)速m/s%RH天氣狀況G1匡口村（園區(qū)內(nèi)）2021.05.0602:00NDNDNDND15.2100.8西南3.672.6多云08:00NDNDNDND20.9100.7西南3.264.7多云14:00NDNDNDND25.7100.6西南2.946.7多云20:00NDNDNDND22.1100.7西南3.558.6多云G2興莊村02:00NDNDNDND15.4100.8西南3.672.8多云08:00NDNDNDND20.9100.7西南3.164.3多云14:00NDNDNDND25.5100.6西南2.846.4多云20:00NDNDNDND22.3100.7西南3.358.3多云G3李巷村02:00NDNDNDND15.4100.8西南3.772.9多云08:00NDNDNDND20.9100.7西南3.264.3多云14:00NDNDNDND25.8100.6西南3.046.4多云20:00NDNDNDND22.3100.7西南3.158.5多云表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目對(duì)二甲苯mg/m3鄰二甲苯mg/m3甲醇mg/m3乙醇mg/m3氣溫℃氣壓kPa風(fēng)向風(fēng)速m/s%RH天氣狀況G1匡口村（園區(qū)內(nèi)）2021.05.0702:00NDNDNDND15.4100.9西3.170.8晴08:00NDNDNDND19.5100.7西2.860.7晴14:00NDNDNDND24.4100.6西2.640.2晴20:00NDNDNDND20.5100.7西2.954.3晴G2興莊村02:00NDNDNDND15.6100.9西3.370.5晴08:00NDNDNDND19.7100.7西2.760.4晴14:00NDNDNDND24.5100.6西2.640.1晴20:00NDNDNDND20.5100.7西3.054.2晴G3李巷村02:00NDNDNDND15.6100.9西3.270.5晴08:00NDNDNDND19.3100.7西2.960.8晴14:00NDNDNDND24.6100.6西2.739.8晴20:00NDNDNDND20.4100.7西2.954.1晴表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目對(duì)二甲苯mg/m3鄰二甲苯mg/m3甲醇mg/m3乙醇mg/m3氣溫℃氣壓kPa風(fēng)向風(fēng)速m/s%RH天氣狀況G1匡口村（園區(qū)內(nèi)）2021.05.0802:00NDNDNDND16.5100.6西南3.768.8晴08:00NDNDNDND22.0100.5西南3.462.4晴14:00NDNDNDND28.6100.4西南3.038.7晴20:00NDNDNDND24.6100.5西南3.556.7晴G2興莊村02:00NDNDNDND16.2100.6西南3.768.7晴08:00NDNDNDND22.2100.5西南3.362.2晴14:00NDNDNDND28.8100.4西南3.138.7晴20:00NDNDNDND24.7100.5西南3.456.5晴G3李巷村02:00NDNDNDND16.3100.6西南3.668.6晴08:00NDNDNDND21.8100.5西南3.362.2晴14:00NDNDNDND28.4100.4西南3.238.9晴20:00NDNDNDND24.6100.5西南3.656.9晴第第25頁(yè)共27頁(yè)表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目對(duì)二甲苯mg/m3鄰二甲苯mg/m3甲醇mg/m3乙醇mg/m3氣溫℃氣壓kPa風(fēng)向風(fēng)速m/s%RH天氣狀況G1匡口村（園區(qū)內(nèi)）2021.05.0902:00NDNDNDND14.5100.7東3.678.9陰08:00NDNDNDND16.8100.6東3.470.6陰14:00NDNDNDND23.6100.5東3.253.6陰20:00NDNDNDND17.4100.6東3.562.3陰G2興莊村02:00NDNDNDND14.2100.7東3.778.6陰08:00NDNDNDND16.7100.6東3.570.2陰14:00NDNDNDND23.4100.5東3.153.1陰20:00NDNDNDND17.3100.6東3.662.7陰G3李巷村02:00NDNDNDND14.6100.7東3.779.2陰08:00NDNDNDND16.6100.6東3.570.1陰14:00NDNDNDND23.8100.5東3.352.9陰20:00NDNDNDND17.5100.6東3.762.5陰表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目對(duì)二甲苯mg/m3鄰二甲苯mg/m3甲醇mg/m3乙醇mg/m3氣溫℃氣壓kPa風(fēng)向風(fēng)速m/s%RH天氣狀況G1匡口村（園區(qū)內(nèi)）2021.05.1002:00NDNDNDND12.5100.8東北3.875.6多云08:00NDNDNDND13.9100.7東北3.469.9多云14:00NDNDNDND20.4100.6東北3.245.6多云20:00NDNDNDND14.7100.7東北3.662.8多云G2興莊村02:00NDNDNDND12.4100.8東北3.774.9多云08:00NDNDNDND13.8100.7東北3.669.5多云14:00NDNDNDND20.4100.6東北3.045.9多云20:00NDNDNDND14.8100.7東北3.862.3多云G3李巷村02:00NDNDNDND12.3100.8東北3.975.8多云08:00NDNDNDND13.7100.7東北3.569.2多云14:00NDNDNDND20.5100.6東北3.245.9多云20:00NDNDNDND14.6100.7東北3.463.2多云表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目對(duì)二甲苯mg/m3鄰二甲苯mg/m3甲醇mg/m3乙醇mg/m3氣溫℃氣壓kPa風(fēng)向風(fēng)速m/s%RH天氣狀況G1匡口村（園區(qū)內(nèi)）2021.05.1102:00NDNDNDND13.0100.9東北3.681.8陰08:00NDNDNDND13.8100.8東北3.472.3陰14:00NDNDNDND16.8100.7東北3.050.6陰20:00NDNDNDND14.6100.8東北3.564.7陰G2興莊村02:00NDNDNDND12.8100.9東北3.581.3陰08:00NDNDNDND13.6100.8東北3.272.8陰14:00NDNDNDND17.2100.7東北2.949.8陰20:00NDNDNDND14.4100.8東北3.464.2陰G3李巷村02:00NDNDNDND13.2100.9東北3.481.4陰08:00NDNDNDND13.9100.8東北3.372.9陰14:00NDNDNDND16.6100.7東北3.050.2陰20:00NDNDNDND14.8100.8東北3.464.1陰表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目對(duì)二甲苯mg/m3鄰二甲苯mg/m3甲醇mg/m3乙醇mg/m3氣溫℃氣壓kPa風(fēng)向風(fēng)速m/s%RH天氣狀況G1匡口村（園區(qū)內(nèi)）2021.05.1202:00NDNDNDND13.4101.0東北2.477.6多云08:00NDNDNDND16.6100.9東北2.370.3多云14:00NDNDNDND20.4100.8東北1.943.7多云20:00NDNDNDND17.0100.9東北2.363.4多云G2興莊村02:00NDNDNDND13.3101.0東北2.676.8多云08:00NDNDNDND16.8100.9東北2.270.7多云14:00NDNDNDND20.3100.8東北2.043.4多云20:00NDNDNDND16.7100.9東北2.463.8多云G3李巷村02:00NDNDNDND13.2101.0東北2.777.2多云08:00NDNDNDND16.2100.9東北2.470.9多云14:00NDNDNDND20.6100.8東北2.043.2多云20:00NDNDNDND17.2100.9東北2.463.9多云表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目鉛及其化合物氣溫℃氣壓kPa風(fēng)向風(fēng)速m/s%RH天氣狀況G1匡口村（園區(qū)內(nèi)）2021.05.06日均值ND21.0100.7西南3.260.7多云G2興莊村日均值ND21.0100.7西南3.260.5多云G3李巷村日均值ND21.1100.7西南3.360.5多云G1匡口村（園區(qū)內(nèi)）2021.05.07日均值ND20.0100.7西2.956.5晴G2興莊村日均值ND20.1100.7西2.956.3晴G3李巷村日均值ND20.0100.7西2.956.3晴G1匡口村（園區(qū)內(nèi)）2021.05.08日均值ND22.9100.5西南3.456.7晴G2興莊村日均值ND23.0100.5西南3.456.5晴G3李巷村日均值ND22.8100.5西南3.456.7晴G1匡口村（園區(qū)內(nèi)）2021.05.09日均值ND18.1100.6東3.466.4陰G2興莊村日均值ND17.9100.6東3.566.2陰G3李巷村日均值ND18.1100.6東3.666.4陰表（4）環(huán)境空氣檢測(cè)結(jié)果表（續(xù)）采樣地點(diǎn)采樣時(shí)間檢測(cè)項(xiàng)目鉛及其化合物氣溫℃氣壓kPa風(fēng)向風(fēng)速m/s%RH天氣狀況G1匡口村（園區(qū)內(nèi)）2021.05.10日均值ND15.4100.7東北3.563.5多云G2興莊村日均值ND15.4100.7東北3.563.2多云G3李巷村日均值ND15.3100.7東北3.563.5多云G1匡口村（園區(qū)內(nèi)）2021.05.11日均值ND14.6100.8東北3.467.4陰G2興莊村日均值ND14.5100.8東北3.367.0陰G3李巷村日均值ND14.6100.8東北3.367.2陰G1匡口村（園區(qū)內(nèi)）2021.05.12日均值ND16.9100.9東北2.263.8多云G2興莊村日均值ND16.8100.9東北2.463.8多云G3李巷村日均值ND16.8100.9東北2.463.8多云以下空白連云港智清環(huán)境科技有限公司連智檢（2021連云港智清環(huán)境科技有限公司連智檢（2021）第164號(hào)第第29頁(yè)共27頁(yè)表（5）土壤檢測(cè)結(jié)果表采樣日期采樣地點(diǎn)T1園區(qū)內(nèi)(德友精工附近)T4園區(qū)內(nèi)采樣深度（cm）0~5000150~150002150~3000030~5000450~150005150~300006檢測(cè)項(xiàng)目單位測(cè)定值2021.05.21pH值無量綱7.87/////陽(yáng)離子交換量cmol+/kg6.0/////氧化還原電位mv510/////容重g/cm31.59/////汞mg/kg0.0680.0480.0300.0710.1250.063砷mg/kg5.234.403.845.102.582.65銅mg/kg65465124299鉛mg/kg19.120.821.014.016.17.2鎳mg/kg412633312214鎘mg/kg0.350.370.430.500.450.27六價(jià)鉻mg/kgNDNDNDNDNDND氯甲烷μg/kgNDNDNDNDNDND氯乙烯μg/kgNDNDNDNDNDND1,1-二氯乙烯μg/kgNDNDNDNDNDND二氯甲烷μg/kgNDNDNDNDNDND反式-1,2-二氯乙烯μg/kgNDNDNDNDNDND1,1-二氯乙烷μg/kgNDNDNDNDNDND順式-1,2-二氯乙烯μg/kgNDNDNDNDNDND氯仿μg/kgNDNDNDNDNDND1,1,1-三氯乙烷μg/kgNDNDNDNDNDND四氯化碳μg/kgNDNDNDNDNDND苯μg/kgNDNDNDNDNDND1,2-二氯乙烷μg/kgNDNDNDNDNDND三氯乙烯μg/kgNDNDNDNDNDND1,2-二氯丙烷μg/kgNDNDNDNDNDND表（5）土壤檢測(cè)結(jié)果表（續(xù)）采樣日期采樣地點(diǎn)T1園區(qū)內(nèi)(德友精工附近)T4園區(qū)內(nèi)采樣深度（cm）0~5000150~150002150~3000030~5000450~150005150~300006檢測(cè)項(xiàng)目單位測(cè)定值2021.05.21甲苯μg/kgNDNDNDNDNDND1,1,2-三氯乙烷μg/kgNDNDNDNDNDND四氯乙烯μg/kgNDNDNDNDNDND氯苯μg/kgNDNDNDNDNDND1,1,1,2-四氯乙烷μg/kgNDNDNDNDNDND乙苯μg/kgNDNDNDNDNDND-二甲苯μg/kgNDNDNDNDNDND鄰二甲苯μg/kgNDNDNDNDNDND苯乙烯μg/kgNDNDNDNDNDND1,1,2,2-四氯乙烷μg/kgNDNDNDNDNDND1,2,3-三氯丙烷μg/kgNDNDNDNDNDND1,4-二氯苯μg/kgNDNDNDNDNDND1,2-二氯苯μg/kgNDNDNDNDNDND苯胺mg/kgNDNDNDNDNDND2-氯苯酚mg/kgNDNDNDNDNDND硝基苯mg/kgNDNDNDNDNDND萘mg/kgNDNDNDNDNDND苯并(a)蒽mg/kgNDNDNDNDNDND?mg/kgNDNDNDNDNDND苯并(b)熒蒽mg/kgNDNDNDNDNDND苯并(k)熒蒽mg/kgNDNDNDNDNDND苯并(a)芘mg/kgNDNDNDNDNDND茚并(1,2,3-cd)芘mg/kgNDNDNDNDNDND二苯并(a,h)蒽mg/kgNDNDNDNDNDND表（5）土壤檢測(cè)結(jié)果表（續(xù)）采樣日期采樣地點(diǎn)T3園區(qū)內(nèi)(云海電源附近)采樣深度（cm）0~5000750~150008150~300009檢測(cè)項(xiàng)目單位測(cè)定值2021.05.21汞mg/kg0.0260.0290.138砷mg/kg1.350.945.59銅mg/kg141518鉛mg/kg20.019.214.2鎳mg/kg221131鎘mg/kg0.310.420.36六價(jià)鉻mg/kgNDNDND氯甲烷μg/kgNDNDND氯乙烯μg/kgNDNDND1,1-二氯乙烯μg/kgNDNDND二氯甲烷μg/kgNDNDND反式-1,2-二氯乙烯μg/kgNDNDND1,1-二氯乙烷μg/kgNDNDND順式-1,2-二氯乙烯μg/kgNDNDND氯仿μg/kg1.41.5ND1,1,1-三氯乙烷μg/kgNDNDND四氯化碳μg/kgNDNDND苯μg/kgNDNDND1,2-二氯乙烷μg/kgNDNDND三氯乙烯μg/kgNDNDND1,2-二氯丙烷μg/kgNDNDND甲苯μg/kgNDNDND1,1,2-三氯乙烷μg/kgNDNDND表（5）土壤檢測(cè)結(jié)果表（續(xù)）采樣日期采樣地點(diǎn)T3園區(qū)內(nèi)(云海電源附近)采樣深度（cm）0~5000750~150008150~300009檢測(cè)項(xiàng)目單位測(cè)定值2021.05.21四氯乙烯μg/kgNDNDND氯苯μg/kgNDNDND1,1,1,2-四氯乙烷μg/kgNDNDND乙苯μg/kgNDNDND-二甲苯μg/kgNDNDND鄰二甲苯μg/kgNDNDND苯乙烯μg/kgNDNDND1,1,2,2-四氯乙烷μg/kgNDNDND1,2,3-三氯丙烷μg/kgNDNDND1,4-二氯苯μg/kgNDNDND1,2-二氯苯μg/kgNDNDND苯胺mg/kgNDNDND2-氯苯酚mg/kgNDNDND硝基苯mg/kgNDNDND萘mg/kgNDNDND苯并(a)蒽mg/kgNDNDND?mg/kgNDNDND苯并(b)熒蒽mg/kgNDNDND苯并(k)熒蒽mg/kgNDNDND苯并(a)芘mg/kgNDNDND茚并(1,2,3-cd)芘mg/kgNDNDND二苯并(a,h)蒽mg/kgNDNDND第第40頁(yè)共27頁(yè)表（6）底泥檢測(cè)結(jié)果表采樣日期采樣地點(diǎn)D1老新莊河閘底泥D2官莊河閘底泥D3200米檢測(cè)項(xiàng)目單位測(cè)定值2021.05.21pH值無量綱8.228.198.20銅mg/kg564947鋅mg/kg174110141鎳mg/kg644757鉻mg/kg128103122鎘mg/kg0.410.380.38鉛mg/kg31.633.229.2汞mg/kg0.0940.0550.032砷mg/kg8.756.347.93樣品性狀/壤土、黃棕色、無異味壤土、黃棕色、微弱壤土、黃棕色、微弱以下空白表（7）包氣帶檢測(cè)結(jié)果表采樣日期采樣地點(diǎn)B1(德友精工附近)B2(北港鎳業(yè)附近)采樣深度地面以下10cm010地下水水位以上20cm011地面以下10cm012地下水水位以上20cm013檢測(cè)項(xiàng)目單位測(cè)定值2021.05.23氟化物mg/L0.560.370.410.40鉛μg/L79.065.243.114.1鉻mg/LNDNDNDND鋅mg/L0.020.050.200.08銅μg/L6.19.06.312.4甲苯μg/LNDNDNDND對(duì)二甲苯μg/LNDNDNDND間二甲苯μg/LNDNDNDND鄰二甲苯μg/LNDNDNDND苯乙烯μg/LNDNDNDND鎳☆μg/L0.7720.1501.601.30經(jīng)度/119°10′38.10″119°10′38.10″119°10′44.56″119°10′44.56″緯度/34°55′3.66″34°55′3.66″34°54′16.32″34°54′16.32″樣品性狀/無植物根系、潮砂壤土、黃棕色無植物根系、濕壤土、棕色無植物根系、潮砂壤土、黃色無植物根系、濕壤土、棕色以下空白表（7）包氣帶檢測(cè)結(jié)果表（續(xù)）采樣日期采樣地點(diǎn)B3(云海電源附近)B4趙沙村(背景值點(diǎn)位)采樣深度地面以下10cm014地下水水位以上20cm015地面以下10cm016地下水水位以上20cm017檢測(cè)項(xiàng)目單位測(cè)定值2021.05.23氟化物mg/L0.440.310.190.13鉛μg/L19966.795.836.0鉻mg/LNDNDNDND鋅mg/L0.09ND0.120.18銅μg/L11.24.311.424.8甲苯μg/LNDNDNDND對(duì)二甲苯μg/LNDNDNDND間二甲苯μg/LNDNDNDND鄰二甲苯μg/LNDNDNDND苯乙烯μg/LNDNDNDND鎳☆μg/L2.341.963.174.37經(jīng)度/119°11′14.68″119°11′14.68″119°10′24.98″119°10′24.98″緯度/34°53′22.76″34°53′22.76″34°55′8.40″34°55′8.40″樣品性狀/無植物根系、潮壤土、黃棕色無植物根系、濕壤土、棕色無植物根系、潮壤土、黃色無植物根系、濕壤土、棕色表（8）噪聲測(cè)量結(jié)果執(zhí)行標(biāo)準(zhǔn)GB3096-2008《聲環(huán)境質(zhì)量標(biāo)準(zhǔn)》測(cè)量時(shí)間2021年05月10日09:22~12:362021年05月10日22:01~05月11日01:152021年05月11日09:17~12:222021年05月11日22:01~05月12日01:25氣象參數(shù)測(cè)點(diǎn)編號(hào)檢測(cè)日期晝間風(fēng)速（m/s）晝間風(fēng)向夜間風(fēng)速（m/s）夜間風(fēng)向檢測(cè)日期晝間風(fēng)速（m/s）晝間風(fēng)向夜間風(fēng)速（m/s）夜間風(fēng)向N12021.05.10~05.113.8東北3.9東北2021.05.11~05.123.4東北3.6東北N23.7東北3.8東北3.5東北3.7東北N33.7東北3.7東北3.6東北3.6東北N43.7東北3.6東北3.4東北3.7東北N53.6東北3.8東北3.5東北3.7東北N63.6東北3.7東北3.4東北3.6東北N73.6東北3.5東北3.5東北3.5東北N83.5東北3.6東北3.5東北3.7東北N93.6東北3.7東北3.4東北3.6東北N103.5東北3.6東北3.6東北3.5東北以下空白噪聲測(cè)量結(jié)果（續(xù)）測(cè)點(diǎn)編號(hào)檢測(cè)點(diǎn)位名稱主要噪聲源等效聲級(jí)LeqdB（A）2021.05.10~05.112021.05.11~05.12晝間夜間晝間夜間N1N1生活噪聲54465548N2N2交通噪聲68536854N3N3生活噪聲53465446N4N4工業(yè)噪聲61506252N5N5生活噪聲55465747N6N6工業(yè)噪聲63516252N7N7工業(yè)噪聲60526353N8N8工業(yè)噪聲62536353N9N9生活噪聲56485848N10N10工業(yè)噪聲53475747備注檢測(cè)期間N2點(diǎn)車輛情況：2021.05.10~05.1185輛/h13815輛/h45輛/h；2021.05.11~05.1283輛/h14718輛/h36輛/h。噪聲校準(zhǔn)表檢測(cè)日期標(biāo)準(zhǔn)值校準(zhǔn)值 dB(A)校準(zhǔn)前校準(zhǔn)后2021.05.1094.093.893.82021.05.1194.093.893.82021.05.1294.093.893.8以下空白附表：土壤參數(shù)表采樣地點(diǎn)采樣深度（cm）采樣日期土壤檢測(cè)點(diǎn)位參數(shù)及樣品性狀統(tǒng)計(jì)表經(jīng)度緯度樣品性狀T1園區(qū)內(nèi)(德友精工附近)0~502021.05.21119°10′42.38″34°55′5.75″無植物根系、潮砂壤土、黃棕色50~150119°10′42.38″34°55′5.75″黃棕色150~300119°10′42.38″34°55′5.75″棕色T4園區(qū)內(nèi)0~50119°11′30.46″34°54′7.16″黃棕色50~150119°11′30.46″34°54′7.16″棕色150~300119°11′30.46″34°54′7.16″灰色T3園區(qū)內(nèi)(云海電源附近)0~50119°11′20.52″34°53′22.76″黃棕色50~150119°11′20.52″34°53′22.76″黃棕色150~300119°11′20.52″34°53′22.76″黃棕色地表水質(zhì)控?cái)?shù)據(jù)統(tǒng)計(jì)表質(zhì)控措施檢測(cè)項(xiàng)目加標(biāo)回收平行值質(zhì)控樣實(shí)驗(yàn)室空白數(shù)量回收率%數(shù)量相對(duì)偏差%保證值測(cè)得值數(shù)量化學(xué)需氧量35.1±1.9（mg/L）35.0（mg/L）35.1±1.9（mg/L）36.5（mg/L）35.1±1.9（mg/L）35.8（mg/L）氟化物//氨氮//總磷6.81±0.73（mg/L）7.16（mg/L）6.81±0.73（mg/L）7.20（mg/L）6.81±0.73（mg/L）7.06（mg/L）鉛//石油類//鉻鋅銅鎳甲苯對(duì)二甲苯間二甲苯鄰二甲苯苯乙烯以下空白海水質(zhì)控?cái)?shù)據(jù)統(tǒng)計(jì)表質(zhì)控措施檢測(cè)項(xiàng)目加標(biāo)回收平行值質(zhì)控樣實(shí)驗(yàn)室空白數(shù)量回收率%數(shù)量相對(duì)偏差%保證值測(cè)得值數(shù)量化學(xué)需氧量氨氮硝酸鹽氮亞硝酸鹽氮活性磷酸鹽六價(jià)鉻石油類以下空白地下水質(zhì)控?cái)?shù)據(jù)統(tǒng)計(jì)表質(zhì)控措施檢測(cè)項(xiàng)目加標(biāo)回收平行值質(zhì)控樣實(shí)驗(yàn)室空白數(shù)量回收率%數(shù)量相對(duì)偏差%保證值測(cè)得值數(shù)量pH值/7.06±0.057.09/鉀/1.54±0.12（mg/L）1.52（mg/L）2鈉/0.882±0.045（mg/L）0.887（mg/L）2鈣/4.48±0.19（mg/L）4.39（mg/L）2鎂/0.118±0.008（mg/L）0.124（mg/L）2總堿度（碳酸根、碳酸氫根）/36.6±2.9（mg/L）37.6（mg/L）2總硬度/1.57±0.23（mmol/L）1.75（mmol/L）2硫酸根/31±1.8（mg/L）32.6（mg/L）2氨氮1//2氯化物/96.4±5.4（mg/L）97.7（mg/L）2耗氧量（CODMn）/13.4±0.8（mg/L）13.8（mg/L）2硝酸鹽氮1//2亞硝酸鹽氮1//2鉛1//2六價(jià)鉻1//2銅1//2鋅1//2甲苯//2對(duì)二甲苯//2間二甲苯//2鄰二甲苯以下空白土壤質(zhì)控?cái)?shù)據(jù)統(tǒng)計(jì)表質(zhì)控措施檢測(cè)項(xiàng)目加標(biāo)回收平行值質(zhì)控樣實(shí)驗(yàn)室空白數(shù)量回收率%數(shù)量相對(duì)偏差%保證值測(cè)得值數(shù)量pH值//5.130±0.1905.16/汞//0.116±0.012（mg/kg）0.110（mg/kg）4砷//13.3±1.1（mg/kg）13.9（mg/kg）4銅//54±2（mg/kg）55（mg/kg）4鉛//41±2（mg/kg）40.2（mg/kg）4鎳//43±2（mg/kg）43（mg/kg）4鎘//0.59±0.04（mg/kg）0.59（mg/kg）4六價(jià)鉻//9.91±0.96（mg/kg）9.78（mg/kg）2陽(yáng)離子交換量//12.5±1.1（cmol+/kg）13.0（cmol+/kg）2氯甲烷2//1氯乙烯2//11,1-二氯乙烯2//1二氯甲烷2//1反式-1,2-二氯乙烯2//11,1-二氯乙烷2//1順式-1,2-二氯乙烯2//1氯仿2//11,1,1-三氯乙烷2//1四氯化碳2//1苯2//11,2-二氯乙烷2//1三氯乙烯2//11,2-二氯丙烷2//1第第50頁(yè)共27頁(yè)土壤、底泥質(zhì)控?cái)?shù)據(jù)統(tǒng)計(jì)表質(zhì)控措施檢測(cè)項(xiàng)目加標(biāo)回收平行值質(zhì)控樣實(shí)驗(yàn)室空白數(shù)量回收率%數(shù)量相對(duì)偏差%保證值測(cè)得值數(shù)量甲苯//11,1,2-三氯乙烷//1四氯乙烯//1氯苯//11,1,1,2-四氯乙烷//1乙苯//1間，對(duì)-二甲苯//1鄰二甲苯//1苯乙烯//11,1,2,2-四氯乙烷//11,2,3-三氯丙烷//11,4-二氯苯//11,2-二氯苯//1苯胺//12-氯苯酚//1硝基苯//1萘//1苯并(a)蒽//1?//1苯并(b)熒蒽//1苯并(k)熒蒽//1苯并(a)芘//1茚并(1,2,3-cd)芘//1二苯并(a,h)蒽//1底泥、包氣帶質(zhì)控?cái)?shù)據(jù)統(tǒng)計(jì)表質(zhì)控措施檢測(cè)項(xiàng)目加標(biāo)回收平行值質(zhì)控樣實(shí)驗(yàn)室空白數(shù)量回收率%數(shù)量相對(duì)偏差%保證值測(cè)得值數(shù)量底泥pH值//21.4/0.15.130±0.1905.16/汞//33.0~5.20.116±0.012（mg/kg）0.110（mg/kg）4砷//30.6~1.613.3±1.1（mg/kg）13.9（mg/kg）4銅//3054±2（mg/kg）55（mg/kg）4鉛//31.0~2.441±2（mg/kg）40.2（mg/kg）4鎳//31.1~4.743±2（mg/kg）43（mg/kg）4鎘//30.6~1.10.59±0.04（mg/kg）0.59（mg/kg）4鉻//1092±4（mg/kg）92（mg/kg）2鋅//11.4127±4（mg/kg）128（mg/kg）2包氣帶氟化物鉛鉻鋅銅甲苯對(duì)二甲苯間二甲苯鄰二甲苯苯乙烯以下空白檢測(cè)方法及儀器一覽表檢測(cè)類別檢測(cè)項(xiàng)目方法依據(jù)檢出限儀器設(shè)備設(shè)備編號(hào)地表水化學(xué)需氧量水質(zhì)化學(xué)需氧量的測(cè)定重鉻酸鹽法HJ828-20174mg/L滴定管ZQ-GW078地表水氟化物水質(zhì)氟化物的測(cè)定離子選擇電極法GB/T7484-19870.05mg/L臺(tái)式PH酸度計(jì)PHSJ-4FZQ-IE031地表水氨氮水質(zhì)氨氮的測(cè)定納氏試劑分光光光度法HJ535-20090.025mg/L可見分光光度計(jì)T6新悅ZQ-IE015地表水總磷水質(zhì)總磷的測(cè)定鉬酸銨分光光度法GB/T11893-19890.01mg/L可見分光光度計(jì)T6新悅ZQ-IE015地表水鉛(第四版增補(bǔ)版)20023.4.16（5）1.0μg/L石墨爐原子吸收分光光度計(jì)TAS-990GZQ-IE013地表水石油類水質(zhì)石油類的測(cè)定紫外分光光度法（試行）HJ970-20180.01mg/L紫外可見分光光度計(jì)T6新世紀(jì)ZQ-IE016地表水六價(jià)鉻水質(zhì)六價(jià)鉻的測(cè)定二苯碳酰二分光光度法 GB/T7467-19870.004mg/L可見分光光度計(jì)T6新悅ZQ-IE015地表水鋅GB/T7475-19870.02mg/L火焰原子吸收分光光度計(jì)TAS-990FZQ-IE012地表水銅(第四版增補(bǔ)版)20023.4.10（5）1.0μg/L石墨爐原子吸收分光光度計(jì)TAS-990GZQ-IE013地表水甲苯水質(zhì)苯系物的測(cè)定頂空/氣相色譜法HJ1067-20192μg/L氣相色譜8890GCZQ-IE005地表水對(duì)二甲苯水質(zhì)苯系物的測(cè)定頂空/氣相色譜法HJ1067-20192μg/L氣相色譜8890GCZQ-IE005地表水間二甲苯水質(zhì)苯系物的測(cè)定頂空/氣相色譜法HJ1067-20192μg/L氣相色譜8890GCZQ-IE005地表水鄰二甲苯水質(zhì)苯系物的測(cè)定頂空/氣相色譜法HJ1067-20192μg/L氣相色譜8890GCZQ-IE005地表水苯乙烯水質(zhì)苯系物的測(cè)定頂空/氣相色譜法HJ1067-20193μg/L氣相色譜8890GCZQ-IE005海水化學(xué)需氧量海洋監(jiān)測(cè)規(guī)范第4部分：海水分析堿性高錳酸鉀法GB17378.4-2007（32）0.15mg/L滴定管ZQ-GW079海水氨海洋監(jiān)測(cè)規(guī)范第4部分：海水分析靛酚藍(lán)分光光度法GB17378.4-2007（36.1）0.0008mg/L可見分光光度計(jì)T6新悅ZQ-IE015檢測(cè)方法及儀器一覽表檢測(cè)類別檢測(cè)項(xiàng)目方法依據(jù)檢出限儀器設(shè)備設(shè)備編號(hào)海水硝酸鹽4GB17378.4-2007（38.1）0.0006mg/L可見分光光度計(jì)T6新悅ZQ-IE015海水亞硝酸鹽4GB17378.4-2007（37）0.0003mg/L可見分光光度計(jì)T6新悅ZQ-IE015海水活性磷酸鹽4GB17378.4-2007（39.1）0.0006mg/L可見分光光度計(jì)T6新悅ZQ-IE015海水六價(jià)鉻水質(zhì)六價(jià)鉻的測(cè)定二苯碳酰二肼分光光度法GB/T7467-19870.004mg/L可見分光光度計(jì)T6新悅ZQ-IE015海水石油類水質(zhì)石油類的測(cè)定紫外分光光度法（試行）HJ970-20180.01mg/L紫外可見分光光度計(jì)T6新世紀(jì)ZQ-IE016地下水鉀水質(zhì)鉀和鈉的測(cè)定火焰原子吸收分光光度法GB/T11904-19890.03mg/L火焰原子吸收分光光度計(jì)TAS-990FZQ-IE012地下水鈉水質(zhì)鉀和鈉的測(cè)定火焰原子吸收分光光度法GB/T11904-19890.010mg/L火焰原子吸收分光光度計(jì)TAS-990FZQ-IE012地下水鈣水質(zhì)鈣和鎂的測(cè)定原子吸收分光光度法GB/T11905-19890.02mg/L火焰原子吸收分光光度計(jì)TAS-990FZQ-IE012地下水鎂水質(zhì)鈣和鎂的測(cè)定原子吸收分光光度法GB/T11905-19890.002mg/L火焰原子吸收分光光度計(jì)TAS-990FZQ-IE012地下水碳酸根《水和廢水監(jiān)測(cè)分析方法》（第四版增補(bǔ)版）國(guó)家環(huán)境保護(hù)總局（2002年）酸堿指示劑滴定法3.1.12（1）5mg/L滴定管ZQ-GW079地下水碳酸氫根（第四版增補(bǔ)版）（2002年3.1.12（1）5mg/L滴定管ZQ-GW079地下水氯化物水質(zhì)氯化物的測(cè)定 硝酸銀滴定法GB/T11896-198910mg/L滴定管ZQ-GW079（F-Cl-NO2-Br-、離子色譜儀CIC-D120地下水硫酸根NO-、PO3-、SO2-、SO2-）3 4 3 40.018mg/LZQ-IE055的測(cè)定離子色譜法HJ84-2016地下水pH值水質(zhì)pH的測(cè)定玻璃電極法GB/T6920-1986—臺(tái)式PH酸度計(jì)PHSJ-4FZQ-IE031地下水耗氧量（CODMn）生活飲用水標(biāo)準(zhǔn)檢驗(yàn)方法有機(jī)物綜合指標(biāo)GB/T5750.7-2006/1.1酸性高錳酸鉀滴定法1.2堿性高錳酸鉀滴定法0.05mg/L電熱恒溫水浴鍋DK-S28ZQ-IE019地下水總硬度水質(zhì)鈣和鎂總量的測(cè)定 滴定法GB/T7477-19875.00mg/L滴定管ZQ-GW079檢測(cè)方法及儀器一覽表檢測(cè)類別檢測(cè)項(xiàng)目方法依據(jù)檢出限儀器設(shè)備設(shè)備編號(hào)地下水溶解性總固體GB/T5750.4-2006/8.1稱量法10mg/L電子天平ATX224ZQ-IE063地下水硝酸鹽氮生活飲用水標(biāo)準(zhǔn)檢驗(yàn)方法無機(jī)非金屬指標(biāo)GB/T5750.5-2006/5.2紫外分光光度法0.2mg/L紫外可見分光光度計(jì)T6新世紀(jì)ZQ-IE016地下水亞硝酸鹽氮水質(zhì)亞硝酸鹽氮的測(cè)定分光光度法GB/T7493-19870.003mg/L可見分光光度計(jì)T6新悅ZQ-IE015地下水氨氮水質(zhì)氨氮的測(cè)定納氏試劑分光光光度法HJ535-20090.025mg/L可見分光光度計(jì)T6新悅ZQ-IE015地下水六價(jià)鉻5750.6-2006/10.1二苯碳酰二肼分光光度法0.004mg/L可見分光光度計(jì)T6新悅ZQ-IE015地下水銅《水和廢水監(jiān)測(cè)分析方法》(第四版增補(bǔ)版)國(guó)家環(huán)境保護(hù)總局2002年石墨爐原子吸收法3.4.10（5）1.0μg/L石墨爐原子吸收分光光度計(jì)TAS-990GZQ-IE013地下水鉛《水和廢水監(jiān)測(cè)分析方法》(第四版增補(bǔ)版)國(guó)家環(huán)境保護(hù)總局2002年石墨爐原子吸收法3.4.16（5）1.0μg/L石墨爐原子吸收分光光度計(jì)TAS-990GZQ-IE013地下水鋅水質(zhì)銅、鋅、鉛、鎘的測(cè)定 原吸收分光光度法GB/T7475-19870.02mg/L火焰原子吸收分光光度計(jì)TAS-990FZQ-IE012地下水甲苯水質(zhì)苯系物的測(cè)定頂空/氣相色譜法HJ1067-20192μg/L氣相色譜8890GCZQ-IE005地下水對(duì)二甲苯水質(zhì)苯系物的測(cè)定頂空/氣相色譜法HJ1067-20192μg/L氣相色譜8890GCZQ-IE005地下水間二甲苯水質(zhì)苯系物的測(cè)定頂空/氣相色譜法HJ1067-20192μg/L氣相色譜8890GCZQ-IE005地下水鄰二甲苯水質(zhì)苯系物的測(cè)定頂空/氣相色譜法HJ1067-20192μg/L氣相色譜8890GCZQ-IE005環(huán)境空氣氨環(huán)境空氣和廢氣氨的測(cè)定納氏試劑分光光度法HJ533-20090.01mg/m3可見分光光度計(jì)T6新悅ZQ-IE015環(huán)境空氣硫化氫（第四版增補(bǔ)版）20030.001mg/m3可見分光光度計(jì)T6新悅ZQ-IE015環(huán)境空氣臭氣濃度空氣質(zhì)量惡臭的測(cè)定三點(diǎn)比較式臭袋法GB/T14675-199310無量綱無臭氣體制備系統(tǒng)ZQ-IE148環(huán)境空氣氯化氫環(huán)境空氣和廢氣氯化氫的測(cè)定離子色譜法HJ549-20160.02mg/m3離子色譜儀CIC-D120ZQ-IE055檢測(cè)方法及儀器一覽表檢測(cè)類別檢測(cè)項(xiàng)目方法依據(jù)檢出限儀器設(shè)備設(shè)備編號(hào)環(huán)境空氣氟化物環(huán)境空氣氟化物的測(cè)定濾膜采樣/氟離子選擇電極法HJ955-20180.5μg/m3臺(tái)式PH酸度計(jì)PHSJ-4FZQ-IE031環(huán)境空氣鉛環(huán)境空氣鉛的測(cè)定石墨爐原子吸收分光光度法HJ539-20150.009μg/m3石墨爐原子吸收分光光度計(jì)TAS-990GZQ-IE013環(huán)境空氣甲苯環(huán)境空氣苯系物的測(cè)定活性炭吸附/二硫化碳解吸-氣相色譜法HJ584-20100.5×10-3mg/m3氣相色譜8890GCZQ-IE005環(huán)境空氣對(duì)二甲苯環(huán)境空氣苯系物的測(cè)定活性炭吸附/二硫化碳解吸-氣相色譜法HJ584-20100.5×10-3mg/m3氣相色譜8890GCZQ-IE005環(huán)境空氣間二甲苯環(huán)境空氣苯系物的測(cè)定活性炭吸附/二硫化碳解吸-氣相色譜法HJ584-20100.5×10-3mg/m3氣相色譜8890GCZQ-IE005環(huán)境空氣鄰二甲苯環(huán)境空氣苯系物的測(cè)定活性炭吸附/二硫化碳解吸-氣相色譜法HJ584-20100.5×10-3mg/m3氣相色譜8890GCZQ-IE005環(huán)境空氣苯乙烯環(huán)境空氣苯系物的測(cè)定活性炭吸附/二硫化碳解吸-氣相色譜法HJ584-20100.5×10-3mg/m3氣相色譜8890GCZQ-IE005環(huán)境空氣硫酸霧固定污染源廢氣硫酸霧的測(cè)定離子色譜法HJ544-20160.002mg/m3離子色譜儀CIC-D120ZQ-IE055環(huán)境空氣甲醇（第四版增補(bǔ)版（2003年）6.1.6(1)0.2mg/m3氣相色譜SP3420AZQ-IE009環(huán)境空氣乙醇《空氣和廢氣監(jiān)測(cè)分析方法》（第四版增補(bǔ)版（2003年）6.1.6(1)0.2mg/m3氣相色譜SP3420AZQ-IE009環(huán)境空氣非甲烷總烴環(huán)境空氣總烴、甲烷和非甲烷總烴的測(cè)定直接進(jìn)樣氣相色譜法HJ604-20170.07mg/m3氣相色譜GC9790IIZQ-IE010土壤pH值土壤pH值的測(cè)定電位法HJ962-2018—臺(tái)式PH酸度計(jì)PHSJ-4FZQ-IE031土壤容重土壤檢測(cè)第4部分:土壤容重的測(cè)定NY/T1121.4-2006—YP系列電子天平Y(jié)P10002ZQ-IE034土壤陽(yáng)離子交換量土壤陽(yáng)離子交換量的測(cè)定三氯化六氨合鈷浸提-分光光度法HJ889-20170.8cmol+/kg可見分光光度計(jì)T6新悅ZQ-IE015土壤氧化還原電位土壤氧化還原電位的測(cè)定電位法HJ746-2015—土壤ORP計(jì)TR-901ZQ-IE176土壤鎘土壤質(zhì)量鉛、鎘的測(cè)定石墨爐原子吸收分光光度法GB/T17141-19970.01mg/kg石墨爐原子吸收分光光度計(jì)TAS-990GZQ-IE013檢測(cè)方法及儀器一覽表檢測(cè)類別檢測(cè)項(xiàng)目方法依據(jù)檢出限儀器設(shè)備設(shè)備編號(hào)土壤汞土壤質(zhì)量總汞、總砷、總鉛的測(cè)定原子熒光法第一部分：土壤中總汞的測(cè)定GB/T22105.1-20080.002mg/kg原子熒光光度計(jì)AFS-8220ZQ-IE003土壤砷土壤質(zhì)量總汞、總砷、總鉛的測(cè)定原子熒光法第二部分：土壤中總砷的測(cè)定GB/T22105.2-20080.01mg/kg原子熒光光度計(jì)AFS-8220ZQ-IE003土壤鉛土壤質(zhì)量鉛、鎘的測(cè)定石墨爐原子吸收分光光度法GB/T17141-19970.1mg/kg石墨爐原子吸收分光光度計(jì)TAS-990GZQ-IE013土壤銅土壤和沉積物銅、鋅、鉛、鎳、鉻的測(cè)定火焰原子吸收分光光度法HJ491-20191mg/kg火焰原子吸收分光光度計(jì)TAS-990FZQ-IE012土壤鎳土壤和沉積物銅、鋅、鉛、鎳、鉻的測(cè)定火焰原子吸收分光光度法HJ491-20193mg/kg火焰原子吸收分光光度計(jì)TAS-990FZQ-IE012土壤六價(jià)鉻土壤和沉積物六價(jià)鉻的測(cè)定堿溶液提取-火焰原子吸收分光光度法HJ1082-20190.5mg/kg火焰原子吸收分光光度計(jì)TAS-990FZQ-IE012土壤四氯化碳土壤和沉積物揮發(fā)性有機(jī)物的測(cè)定吹掃捕集/氣相色譜-質(zhì)譜法HJ605-20111.3μg/kg氣質(zhì)聯(lián)用儀8890-5977BZQ-IE008土壤氯仿土壤和沉積物揮發(fā)性有機(jī)物的測(cè)定吹掃捕集/氣相色譜-質(zhì)譜法HJ605-20111.1μg/kg氣質(zhì)聯(lián)用儀8890-5977BZQ-IE008土壤氯甲烷土壤和沉積物揮發(fā)性有機(jī)物的測(cè)定吹掃捕集/氣相色譜-質(zhì)譜法HJ605-20111.0μg/kg氣質(zhì)聯(lián)用