凍干機(jī)手動和自動操作指引

1、5.1. Freeze-dryingOperation操作用戶操作設(shè)備進(jìn)行凍干程序操作Loggingincontrolsystemisneededbeforeoperatingtheequipment.Inthecontrolsystem,freeze-dryingprocesscanbedonethrough2methods.操作用戶若需要對設(shè)備進(jìn)行操作需要先登入控制系統(tǒng)。在控制系統(tǒng)中對于凍干可通過2種方式來完成AutomaticControl自動控制ManualControl手動控制5.1.1 Operatorrunsautomaticcontroltodofreeze-dryingope

2、ration操作用戶運行自動控制進(jìn)行凍干流程操作Inautomaticcontrol,switchallthecontrolcomponentstoautomaticcontrolstatusatfirstandthensettherecipeparameters.Afterthat,will'aplpARTAUTO.Userclicksthe“STARTAUTO.buttontostartautomaticprogram.在自動控制中需要先切換把所有的控制部件切換到自動控制狀態(tài)，然后設(shè)置配方參數(shù)，當(dāng)設(shè)置好配方參數(shù)后開始自動”按鈕會顯示，用戶點擊開始自動”按鈕啟動自動程序。Contro

3、lcomponentsopenandcloseautomaticallyaccordingtoautomaticprogram.Atthemeanwhile,statusof“AUTOontherightuppercornerwillbecomegreenandtheinterfaceswitchbutton“FREZE_DRYINGontheleftlowercornerwillalsohassmallgreenframe.自動程序運行后控制部件按程序自動運行開啟和關(guān)閉，同時在界面右上角的”自動”狀態(tài)會顯示綠色、左下角的凍干”界面切換按鈕也會有綠的小方框顯示。Theoperationstat

4、usofautomaticprogramcanbedisplayedbyclickingthe“Probuttononrightlowerpartandswitchingtoprogramoperationalstatus.自動程序的運行狀況可點擊界面右下部分的程序”按鈕切換到程序運行狀態(tài)顯示。5.1.2 ControlComponentsSwitchtoAutomaticControlStatus控制部件切換到自動控制狀態(tài)Clickanycontrolcomponentsontheinterfaceanddigitalsignatureofcomponentscontrolwillpopup

5、.Afterenteringtheusernameandpassword,componentcontrolpicturewillappear.Click“ALLTHECOMPONENTSCHANGETOAUTObesidecomponentspictureontheMODEbuttonandallthecomponentscontrolturntoautomaticmodel.Userscanfindoutstatusswitchfromthestatusiconinterface.點擊界面的任何控制部件會彈出部件控制的電子簽名，輸入操作用戶和密碼后顯示部件的控制畫面，點擊”全部切換為自動”按

6、鈕后所有的控制部件切換為自動模式，用戶可從界面部件畫面旁的狀態(tài)圖標(biāo)可看出狀態(tài)的切換5.1.3 RecipeParametersSetting設(shè)置配方參數(shù)Beforerunningtheautomaticprograms,recipeparametersshouldbesetanddownloadedtothePLCinordertoruntheprogramaccordingtodesignedprocess.Ifaboveoperationwillnotbedone,“STARTAUTO.buttospwiyandautomaticprogramwillnotstart.在運行自動程序前需要

7、設(shè)定配方參數(shù)并且下載到可編程控制器里（PLC）以讓程序按設(shè)好的工藝進(jìn)行運行，若不進(jìn)行上述操作則自動”按鈕不會顯示，自動程序也將無法啟動。1. .OperationButtons操作按鈕No.ButtonName按鈕名稱ButtonInstructions按鈕說明1View查看Viewtherecipe配方的查看2Modify修改Modifytherecipe配方的修改3New新建Buildnewrecipe,newrecipenameshouldbeenteredbeforebuilding配方的新建，在新建配方前需要輸入新配方名4Save保存Savetherecipe.Relevantrec

8、ipesshouldbesavedinthecomputeraftermodificationforfreeze-dryingoperationatnexttime.配方的保存，在修改配方后需要對相應(yīng)的配方進(jìn)行保存操作，保存到電腦系統(tǒng)中以供下次凍干操作使用5Download下載Recipedownloading.DownloadtherecipetoPLCinordertoprovideparametersforautomaticprogramrunningoffreeze-drying.配方的下載，使配方數(shù)掂下載到可編程控制器里供凍干自動程序運行提供參數(shù)。6Print打印Printingth

9、erecipethroughprinteroutput配方的打印，通過打印機(jī)輸出7Delete刪除Deletetherecipe.Thisoperationisnotadvisedevenunreasonablerecipeexists.配方的刪除，此操作不建議使用，即使啟/、合理的配方也不建議刪除操作2. ParametersInstruction參數(shù)說明Controlprocessoffreeze-dryingisdividedinto4partsincludingFreezingControl(ProgramSection16),CondenserFreezing(ProgramSect

10、ion7,8),PrimaryDrying(ProgramSection919),andDryingAnalysis(ProgramSection2023).The9thstepsectioninPrimaryDryingispre-vacuumizingphaseandinthisphasewarming-upcontrolwillnotbedone.Thetemperaturetobesetshouldbeconsistentwiththetemperaturesettingvalueinthe6thstepsection.Eachstepsectioncanincludetemperat

11、uresetting,vacuumsetting,andvacuumcontrolchoiceandpressure-upcontrolchoiceaccordingtocontrolrequirements.冷凍干燥控制流程分為4部分包括預(yù)冷(程序段16段)、后箱冷卻(程序段7、8段)、第一次升華干燥(程序段919段)、解析干燥(程序段2023段)，升華干燥中的第9步段是預(yù)抽真空的階段，此階段不進(jìn)行升溫控制，設(shè)置的溫度需要和第6步段的溫度設(shè)定值一致，每個步段按控制需求可包括溫度設(shè)置、真空設(shè)置、真空控制選擇和壓力升控制選擇。FreezingControlpartdoesnotincludeva

12、cuumsetting,vacuumcontrolchoiceandpressure-upcontrolchoice.The7thstepsectioninCondenserFreezingpartiscondensertemperaturesettingandthe8thstepsectionismaintainingtimeaftercondensertemperatureisreached(atleastset20min).預(yù)冷部分不包含真空設(shè)置、真空控制選擇和壓力升控制選擇。后箱冷卻部分第7步段是后箱溫度設(shè)置，第8步段是達(dá)到后箱溫度后維持的時間(至少設(shè)置20分鐘)。The9thstep

13、sectioninPrimaryDryingispre-vacuumizingphaseandinthisphasewarming-upcontrolwillnotbedone.Thetemperaturetobesetshouldbeconsistentwiththetemperaturesettingvalueinthe6thstepsection.Ifchoosepressure-upcontrolbuttoninthe19thstepsection,thepressure-upcontrolwillstartsafterthe19thstepsectionandthiscontroli

14、ncludes2parametertesttimeandpressure-upsettingvalue.升華干燥中的第9步段是預(yù)抽真空的階段，此階段不進(jìn)行升溫控制，設(shè)置的溫度需要和第6步段的溫度設(shè)定值一致，若在第19步段行若選擇壓力升控制選擇按鈕，則在19步段結(jié)束后進(jìn)行壓力升控制，壓力升控制包括2個參數(shù):測試時間和壓力開設(shè)定值。AsthesamewithPrimaryDrying,ifchoosepressure-upcontrolinthe23thstepsectioninDryingAnalysispart,thecontrolwillstartsafterthe23thstepsecti

15、onandthatcontrolincludes2parametertesttimeandpressure-upsettingvalue.解析干燥部分和升華干燥一樣若在第23步段行若選擇壓力升控制選擇按鈕，則在23步段結(jié)束后進(jìn)行壓力升控制，壓力升控制包括2個參數(shù)：測試時間和壓力升設(shè)定值。5.1.4 AutomaticProgramStart自動程序啟動UserclicksAftersettingtherecipeparameters,“STARTAUTO.buttonwillappears.the“STARTAUTO.buttontostartautomaticprogram.當(dāng)設(shè)置好配方參數(shù)

16、后開始自動”按鈕會顯示，用戶點擊開始自動”按鈕啟動自動程序。5.1.5 ProcessStatusInquiry>ParameterModificationandForcedComponentControl過程狀態(tài)的查詢、參數(shù)修改和部件強制控制RecipeParameter配方參數(shù)ControlParameter控制參數(shù)OperationParameter運行參數(shù)T討工，I爆郵d討4功自功D.ocn尊阪二事統(tǒng)瞥書，手聲出日：配方君!4力*岡AcnVLtMilVIirFiR賓主融止SRTS"Erzr星5"we已W.卡口T"Iff內(nèi)區(qū)三甲7|二必口韶|e吐山電擊

17、也H片號才壓力信號F>!KFlr1OJnJji1!2七min.iiSOJO七I14GUOpuZinJ5MrJTdHJ*OJO七0nin.寸|詐印再通市（聃*時閩防«巾苒空m幗用母力瑁啊生理后推抬卻!00t0103式"斜QJ0VO.M»E±-1Fnin1jiJF-H帕iziMrtuu.iM*MMDElb4Eimln13-QQotcoipt4FminOJl弋,OO杜血1cja1止.gyq叩iztu.niiL-1。O"0MBiMil1Mt0*叩EtNTVran.;哈rarv也城吐就nrDdn1NM七0.M0述stQiliai靜所干找，KDflp

18、y21JL七Q.MQ4rp，23OJO弋OUDDc±ii1nib1：.力一-*廿州-小fli±-,9mu卜地七/Mi凡-T1*1七'自濯君打過現(xiàn)狀志a示！七110.100Efcar*苴01OldOd>4!E竽包叱明1o.mi.»IO.D免*帛VMEUAF1iHESAtBl0WZ然iirtilFT10M8M1/ITiiy1niri1njFiTflsn*o；o禹一r-!1r-!1rB!TI：3PTB.ftffiSTfl1pvjtfjiiraiJPU，_H，B件flRunningstatusduringautomaticprogramoperationca

19、nbedisplayedbyclickingthe“Program“buttonatrightlowerpartofinterfaceandswitchingtoprogramrunningstatusastheabovepicture.自動程序運行時的運行狀況可點擊界面右下部分的程序”按鈕切換到程序運行狀態(tài)顯示，如上圖Interfaceparametermainlyconsistsofrecipeparameter,controlparameterandoperationparameter.界面參數(shù)主要分3部分組成，配方參數(shù)、控制參數(shù)和運行參數(shù)。5.1.6 RecipeParameter己方

20、參數(shù)RecipeParameteristhemaintechnicalparameteroffreeze-dryingoperation.Ifonlywanttomodifythetechnicaldataofcurrentbatchduringoperation,usercandosomesettingsatthisinterface.Exceptthedataoffirststepsectioncannotbemodifiedafterautomaticprogramstarting,otherdatacanallbemodifiedduringtheoperation.Pleasesee

21、thehapterofsettingrecipeparametersfordetailinformation.配方參數(shù)是冷凍干燥運行的主要工藝參數(shù)，在運行過程中若只希望修改本批次運行的工藝數(shù)據(jù)可在此界面進(jìn)行設(shè)置。除第1步段的數(shù)據(jù)在自動程序運行后不能修改，其他的數(shù)據(jù)在運行過程中均可修改。詳細(xì)說明請見設(shè)置配方參數(shù)章節(jié)。5.1.7 ControlParamete控制參數(shù)ControlParameterisaccessoryparameterofautomaticprogramoperationbesidesthetechnicalrecipeparameter.Itsinstructionisasf

22、ollow:控制參數(shù)是除工藝配方參數(shù)以外自動程序運行的輔助參數(shù)，說明如下表。NO.ParameteEtems#數(shù)項Instruction說明1TEMP.CONTROLDEVIATION溫度控制上偏差Upperdeviationofparameterprecisioncontroloftemperaturesetting溫度設(shè)置參數(shù)精度控制上偏差2TEMP.CONTTOLDEVIATION(L)溫度控制下偏差Lowerdeviationofparameterprecisioncontroloftemperaturesetting溫度設(shè)置參數(shù)精度控制下偏差3VACCONTDEVIATION真空控制

23、上偏差Upperdeviationofparameterprecisioncontrolofvacuumsetting真空設(shè)置參數(shù)精度控制上偏差4VACCONTDEVIATION(L)真空控制下偏差Lowerdeviationofparameterprecisioncontrolofvacuumsetting真空設(shè)置參數(shù)精度控制下偏差5VACALARMVALUE真空報警設(shè)定值Vacuumalarmparameter.IfchambervacuumhigherthanthissettingvalueduringPrimaryDryingoperation,theheatingcontrolwil

24、lbeclosedandcoolingwillbedonetothechamber.Whenvacuuminthechamberislowerthanthesettingvacuumvalue,heatingcontrolwillrestarts.真空報警參數(shù)，升華干燥階段運行后若前箱真空高于此設(shè)定值則加熱控制關(guān)閉，同時對前箱進(jìn)行制冷，當(dāng)箱內(nèi)真空低于配方設(shè)定真空值則恢復(fù)加熱控制6PID_CYCLEPID周期設(shè)定值PIDControlCirculationCyclePID控制循環(huán)周期7PID_ACCURACYPID精度設(shè)定值PIDControlAccuracyPID控制精度8PID_PROPOR

25、TIONPID比例設(shè)定值PIDControlProportionParametersPID控制比列參數(shù)9PID_INTEGRALPID積分設(shè)定值PIDControlIntegralParametersPID控制積分參數(shù)10PID_DIFFERENTIALPID微分參數(shù)設(shè)定值PIDControlDifferentialParametersPID控制微分參數(shù)OperationParameter運行參數(shù)OperationParameterisstatusdisplayduringautomaticprogramoperatingperiod.Detaildisplayisasfollow:運行參數(shù)是

26、自動程序運行過程中的狀態(tài)顯示，具體顯示如下圖No.ParameteEtem參數(shù)項Instruction說明1RUNNINGSTEP運行步段號Numberofrunningstepsection運行的步段號2RUNNINGSECTION步段說明Instructionofrunningstepsection運行步段的說明3TEMP.SELECT溫度設(shè)定值Temperaturesettingvalueofrunningstepsection運行步段的溫度設(shè)定值4TEMP.OILINLET導(dǎo)熱油進(jìn)口溫度Temperaturerunningvalueofrunningstepsection運行步段的溫度

27、運行值5VAC.SELECT真空度設(shè)定值Vacuumsettingvalueofrunningstepsection運行步段的真空設(shè)定值6VAC.CHAMBER箱內(nèi)真空度Vacuumrunningvalueofrunningstepsection運行步段的真空運行值7TIMESELECT步段時間設(shè)定值Timsettingvalueofrunningstepsection運行步段的時間設(shè)定值8TIMERUNNINGSELECT步段時間運行值Timrunningvalueofrunningstepsection運行步段的時間運行值5.1.8 AutomaticProgramStop自動程序停止Au

28、tomaticprogramstopsinsequence,andindicatinglightofelectricitycabinetwillturngreenforindication.Userclicks“STOPAUTO.buttontostopautomaticprogram.自動程序按順序運行結(jié)束，電氣柜的指示燈會亮綠燈指示，用戶點擊停止自動按鈕停止自動程序。5.1.9 Userrunsmanualcontroltodofreeze-dryingoperation操作用戶運行手動控制進(jìn)行凍干流程操作Userscanmanuallycontrolcomponentsinthesyst

29、emduringmanualcontrol(automaticcontroldoesnotrun).Forthesamecomponent,thereare3kindsofbuttonsforoperationcontrol.在手動過程中(自動控制沒有運行)用戶可對系統(tǒng)中的部件進(jìn)行手動控制。對同一個部件有3種按鈕進(jìn)行操作控制。Manual:thisoperationcanforcedlystartthecontrolcomponents;手動：操作可強制開啟控制部件Automatic:thisoperationcanmakecontrolcomponentsjoininautomaticlog

30、icalcontrolduringautomaticoperation;自動：在自動運行過程中使控制部件參與自動邏輯控制Stop:thisoperationcanstoptheopencontrolcomponents.停止：操作可停止開啟的控制部件ManualControl_lllWillbedisplayedbesidethecontrolcomponentafteroperation部件手動控制操作結(jié)束在控制部件旁顯AllcomponentsturntoautomaticcontrolWillbedisplayedbesideallcontrolcomponentsafteroperat

31、ion部件全部切換自動控制操作結(jié)束在所有控制部件旁AutomaticControlStopControlWillbedisplayedbesidecontrolcomponentafteroperation部件停止控制操作結(jié)束在控制部件Note：Inmanualcontrol,openvacuumpumpmorethan20minbeforeopeningthesmallbutterflyvalve.注：在手動控制下，開啟小蝶閥前先要開啟真空泵20分鐘以上。Exceptthemanualcomponentcontrol,otherfunctionalcontrolsareneededtomee

32、tthenormaltechnicalrequirementsofautomaticprogram.Theyareasfollow:除手動部件控制外若要保證自動程序的正常工藝需求，還需要其他的功能控制的參與，見下表No.ControlItem控制項Instruction說明1TEMPCONTROL溫度控制Circulationpumpstarts,HEATINGCONTROLcanberunifthevacuumisnormal.循環(huán)泵開啟，真空止常則可進(jìn)行加熱控制IfOILINLETTEMP>HEATINGTEMP.(C)beforetemperaturecontrolstarts,h

33、eatingcontrolwillstarts.溫度控制啟動前若導(dǎo)熱油進(jìn)口溫度>加熱設(shè)定溫度(C)則進(jìn)行加熱控制。PIDtemperaturecontrolanddeviationalarmingtreatmentaredonetotheheater.Ifthetemperatureistoohigh-OILINLETTEMP>HEATINGTEMP.(C)+TEMP.Colddopingvalvewillopen.加熱器進(jìn)行PID溫度控制并且進(jìn)行偏差報警處理，溫度開的太高，導(dǎo)熱油進(jìn)口溫度>加熱設(shè)定溫度(C)+偏差溫度則摻冷閥打開。CONTROLDEVIATION,coldd

34、opingvalvewillopenandchambertemperaturegoesdown.WhenOILINLETTEMP<HEATINGTEMP.(C),colddopingvalvewillclose.控制偏差則摻冷閥打開，止匕時前箱隔板溫度降低，當(dāng)導(dǎo)熱油進(jìn)口溫度<加熱設(shè)定溫度(C),摻冷閥關(guān)閉。IfOILINLETTEMP<HEATINGTEMP.(C)beforetemperaturecontrolstarts,coolingcontrolwillbedoneandheaterandcolddopingvalvewillnotattendthecontrol.溫

35、度控制啟動前若導(dǎo)熱油進(jìn)口溫度<加熱設(shè)定溫度(C)則進(jìn)行制冷控制。加熱器、摻冷閥/、參與控制。IfOILINLETTEMP>HEATINGTEMP.(C)+TEMP.CONTROLDEVIATION,platecoolingvalveopensandcondensationvalvecloses,temperatureofchamberisolatingplategoesdown.導(dǎo)熱油進(jìn)口溫度>加熱設(shè)定溫度(C)+溫度控制偏差，則板冷閥打開冷凝閥關(guān)閉，止匕時前箱隔板溫度降低。WhenOILINLETTEMP<HEATINGTEMP.(C),condensationval

36、veopensandplatecoolingvalvecloses.當(dāng)導(dǎo)熱油進(jìn)口溫度<加熱設(shè)定溫度(C)則冷凝閥打開板冷閥關(guān)閉。2VAC.CONTROL真空控制Thesameastemperaturedeviationcontrol,whenCHAMBERVACUUM<VACUUMCONTROLSELECT(Pa)-VACCONTDEVIATIONduringfreeze-dryingprocess,aerificationvalvewillopen.AndifCHAMBERVACUUM>VACUUMCONTROLSELECT(Pa)+VACCONTDEVIATION(L),

37、theaerificationvalvewillclose.和溫度的偏差控制一樣，冷凍干燥運行過程中箱內(nèi)真空值<真空控制設(shè)定值(Pa)-真空偏差值，則摻氣閥打開-箱內(nèi)真空值,真空控制設(shè)定值(Pa)+真空偏差值，則摻氣閥關(guān)閉。3VAC.ALARM真空報警CHAMBERVACUUM>VAC.ALARMCONTROL,heatingcontrolclosesandalarmingstarts.CHAMBERVACUUM<EVACUATIONCONTROL(Pa),Alarmdisable.箱內(nèi)真空度,報警真空設(shè)定值，則加熱控制關(guān)閉，同時報警提示，箱內(nèi)真空度<疏散控制設(shè)定值(P

38、a),則報警解除。5TAMPONADEAfterfreeze-dryingprogram,TAMPONADECONTROLcanbeCONTROL壓塞控制started.Tamponadecontrolofhydraulicpressuredeclinewillstartautomatically.WhenSHELFPRESSWITCHsignalisjudged,hydraulicpressurecontrolstopsandTAMPONADECONTROLends.在凍干程序結(jié)束后可進(jìn)行壓塞控制，液壓自動啟動下降進(jìn)行壓塞，當(dāng)判斷壓塞控制信號后液壓控制停止壓塞結(jié)束SettingParamet

39、ersofManualOperationforCoolingContro泠凍控制手動運行設(shè)定參數(shù)NO.ControlItems控制項Instruction說明1HEATINGTEMP.(C):加熱溫度設(shè)定值SettingValueofTemperatureControl溫度控制設(shè)定值2HEATINGTIME(Min)加熱時間設(shè)定值TemperatureControlTime溫度控制時間3EVACUATIONCONTROL(Pa)真空控制設(shè)定值SettingValueofVacuumAlarm真空控制設(shè)定值4ALARMCONTROL真空報警設(shè)定值Vacuumalarmingparameter.W

40、henchambervacuumishigherthanthissettingvalueduringPrimaryDryingprocess,heatingcontrolcloseandalarmstarts.真空報警參數(shù)，升華階段運行后若前箱真空高于此設(shè)定值則加熱控制關(guān)閉，同時報警提示5TEMP.CONTROLDEVIATION溫度控制上偏差Upperdeviationofparameterprecisioncontroloftemperaturesetting溫度設(shè)置參數(shù)精度控制上偏差6TEMP.CONTTOLDEVIATION(L)溫度控制下偏差Lowerdeviationofparam

41、eterprecisioncontroloftemperaturesetting溫度設(shè)置參數(shù)精度控制下偏差7VACCONTDEVIATION真空控制上偏差Upperdeviationofparameterprecisioncontrolofvacuumsetting真空設(shè)置參數(shù)精度控制上偏差8VACCONTDEVIATION(L)真空控制下偏差Lowerdeviationofparameterprecisioncontrolofvacuumsetting真空設(shè)置參數(shù)精度控制下偏差Useroperatesequipmenttododeicingprogram操作用戶操作設(shè)備進(jìn)行化霜程序操作Operatingusersshouldloginthecontrolsystemfirstlyiftooperatetheequipment.Deicingcanbecompletedby1meth