級(jí)醇溶粘結(jié)性直焊聚酯漆包銅圓線

1、 Q/321181 RLH 002-2013 K12 Q丹陽利華電子有限公司企業(yè)標(biāo)準(zhǔn) Q/321181 RLH 002-2013 130級(jí)醇溶粘結(jié)性直焊聚氨酯漆包銅圓線2013 - - 發(fā)布 2013 - - 實(shí)施 丹陽利華電子有限公司 發(fā)布前 言本產(chǎn)品由于具有特殊的專業(yè)要求（如醇溶粘結(jié)等），而此粘結(jié)試驗(yàn)沒有相應(yīng)的國家標(biāo)準(zhǔn)和行業(yè)標(biāo)準(zhǔn)，為確保 產(chǎn)品質(zhì)量，規(guī)范市場(chǎng)，根據(jù)中華人民共和國標(biāo)準(zhǔn)的規(guī)定，特制定標(biāo)準(zhǔn)，作為組織生產(chǎn)和檢驗(yàn)的依據(jù)。 本標(biāo)準(zhǔn)漆包線試驗(yàn)方法按國家標(biāo)準(zhǔn)GB/T4074-2008執(zhí)行。本標(biāo)準(zhǔn)按照GB/T1.1-2009標(biāo)準(zhǔn)化工作導(dǎo)則第1、第2部分：標(biāo)準(zhǔn)的結(jié)構(gòu)和編寫進(jìn)行編寫。本標(biāo)準(zhǔn)有丹陽利

2、華電子有限公司提出并負(fù)責(zé)起草。本標(biāo)準(zhǔn)起草人：方澄秋本標(biāo)準(zhǔn)于 年 月 日 首次發(fā)布I130級(jí)醇溶粘結(jié)性直焊聚氨酯漆包銅圓線1、 范圍本標(biāo)準(zhǔn)規(guī)定了130級(jí)醇溶粘結(jié)性直焊聚氨酯漆包銅圓線的產(chǎn)品分類、技術(shù)要求、試驗(yàn)方法、檢測(cè)規(guī)則、標(biāo)志、包裝、運(yùn)輸及貯存。本標(biāo)準(zhǔn)適用于130級(jí)醇溶粘結(jié)性直焊聚氨酯漆包銅圓線。產(chǎn)品主要用于制造傳聲器、揚(yáng)聲器音圈及其它需要在低溫粘結(jié)成型的特種線圈。2、 規(guī)范性引用文件下列文件中的條款通過本標(biāo)準(zhǔn)的引用而成為本標(biāo)準(zhǔn)條款。凡是注日期為引用文件，其隨后所有的修改單（不包括勘誤的內(nèi)容）或修訂版均不適用于本標(biāo)準(zhǔn)。然而，鼓勵(lì)根據(jù)本標(biāo)準(zhǔn)達(dá)成協(xié)議的各方研究是否可使用這些文件的最新版本。凡是不注

3、日期的引用文件，其最新版本適用于本標(biāo)準(zhǔn)。IEC 60317-2（1990）130級(jí)粘結(jié)性直焊聚氨酯漆包銅圓線JISC 32021994 自粘性聚氨酯漆包線GB/T 6109.9-89 熱粘合或溶劑粘合直焊性聚氨酯漆包圓銅線GB/T 6108.22003 繞組線基本尺寸GB/T 4074.1-4074.6-2008 繞組線試驗(yàn)方法JB/T 8135.2-1997 繞組線線盤包裝3、產(chǎn)品分類3.1、使用特性3.1.1、漆包線具有醇溶性自粘層，溶于工業(yè)無水乙醇（C2H5OH含量99.9%），乙醇揮發(fā)后，該自粘層即具有一定的粘結(jié)力，使線圈成型。該自粘層且能與聚乙烯、聚酰胺樹脂膠水互融、互粘。3.1.2

4、、在普通大氣壓下未經(jīng)浸漬處理的漆包線，20000小時(shí)外推壽命不低于130，產(chǎn)品的熱級(jí)為B（130）。3.2、型號(hào)和產(chǎn)品表示方法3.2.1、型號(hào) QAN/130/YQAN聚氨酯型自粘漆包銅圓線130溫度指數(shù)值Y音圈用3.2.2、產(chǎn)品表示方法產(chǎn)品型號(hào)、導(dǎo)體標(biāo)準(zhǔn)直徑及本標(biāo)準(zhǔn)編號(hào)三部分組成。示例 標(biāo)稱直徑0.06mm的130級(jí)醇溶粘結(jié)性直焊聚氨酯漆包銅圓線，表示為QAN/130/Y 0.064、 技術(shù)要求4.1、技術(shù)要求應(yīng)符合表1的規(guī)定表1序號(hào)項(xiàng)目名稱技術(shù)要求試驗(yàn)型式試驗(yàn)方法1表面質(zhì)量符合本標(biāo)準(zhǔn)第4.3條規(guī)定T.R按本標(biāo)準(zhǔn)5.3執(zhí)行2尺寸2.1導(dǎo)體尺寸符合本標(biāo)準(zhǔn)第4.4條規(guī)定T.RGB/T 4074.

5、22.2漆包線外徑3電阻符合本標(biāo)準(zhǔn)第4.4條規(guī)定T.SGB/T 4074.24伸長(zhǎng)率符合本標(biāo)準(zhǔn)第4.4條規(guī)定T.SGB/T 4074.35柔韌性和附著性5.1卷繞符合本標(biāo)準(zhǔn)第4.5.1條規(guī)定T.SGB/T 4074.35.2急拉斷符合本標(biāo)準(zhǔn)第4.5.2條規(guī)定6回彈性符合本標(biāo)準(zhǔn)第4.6條規(guī)定T.SGB/T 4074.37熱沖擊符合本標(biāo)準(zhǔn)第4.7條規(guī)定T.SGB/T 4074.68軟化擊穿符合本標(biāo)準(zhǔn)第4.8條規(guī)定T.SGB4/T 074.69擊穿電壓符合本標(biāo)準(zhǔn)第4.9條規(guī)定T.SGB/T 4074.510常態(tài)針孔符合本標(biāo)準(zhǔn)第4.10條規(guī)定T.S按本標(biāo)準(zhǔn)5.4執(zhí)行11焊錫性符合本標(biāo)準(zhǔn)第4.11條規(guī)定

6、T.SGB/T 4074.412粘結(jié)強(qiáng)度12.1不發(fā)粘性符合本標(biāo)準(zhǔn)第4.12.1條規(guī)定T.S按本標(biāo)準(zhǔn)5.5.1執(zhí)行12.2粘結(jié)強(qiáng)度符合本標(biāo)準(zhǔn)第4.12.2條規(guī)定13耐溶劑符合本標(biāo)準(zhǔn)第4.13條規(guī)定T.SGB/T4074.414耐藥品性符合本標(biāo)準(zhǔn)第4.14條規(guī)定T.S按本標(biāo)準(zhǔn)5.6執(zhí)行15包裝符合本標(biāo)準(zhǔn)第7條規(guī)定R目力檢查 注：T型式檢驗(yàn) S抽樣檢驗(yàn) R例行檢驗(yàn)4.2、材料4.2.1、漆包線的銅導(dǎo)體應(yīng)符合GB/T 6108.22003繞組線基本尺寸其直徑的允許偏差應(yīng)符合表2的規(guī)定。4.2.2、漆包線用漆應(yīng)滿足本標(biāo)準(zhǔn)其制造的漆包線規(guī)定的各項(xiàng)性能要求。4.3、表面質(zhì)量漆包線表面應(yīng)光滑、色澤均勻，在常

7、溫下漆包線之間不粘結(jié)，漆膜堅(jiān)韌，即用手指甲尖刮劃時(shí)，漆膜不剝離。4.4、尺寸、伸長(zhǎng)率、電阻值漆包線的尺寸、伸長(zhǎng)率、電阻應(yīng)符合表2的規(guī)定。導(dǎo)體的不圓度f值不大于導(dǎo)體直徑偏差的絕對(duì)值。4.5、柔韌性和附著性4.5.1、從同一線軸上取約長(zhǎng)350mm的試樣3根，在試驗(yàn)上分別標(biāo)出距離為200mm的標(biāo)線，以每分鐘360mm以下的拉伸速度拉伸到斷，用約15倍的放大鏡檢查，漆膜應(yīng)不開裂。4.5.2、漆包線急拉斷后，漆膜應(yīng)不開裂或失去附著性。表2 自粘線尺寸、伸長(zhǎng)率、電阻值要求表單位（mm）導(dǎo)體1種class12種class23種class3最小伸長(zhǎng)率%導(dǎo)體電阻/m直徑公差最小絕緣厚度最小自粘層厚度最大成品外徑

8、最小絕緣厚度最小自粘層厚度最大成品外徑最小絕緣厚度最小自粘層厚度最大成品外徑最小最大0.0200.001-0.00150.0010.0300.00150.0010.026754.6855.780.0250.002-0.0020.00150.0370.0020.00150.033734.7935.920.0300.002-0.0020.0020.0440.0020.0020.039824.2224.880.0350.002-0.0020.0020.0480.0020.0020.045817.8318.240.0400.0020.0030.0030.0600.0020.0020.0560.0020

9、.0020.050913.6713.950.0450.0020.0030.0030.0670.0020.0020.0600.0020.0020.055910.8111.010.0500.0020.0040.0030.0720.0030.0020.0690.0030.0020.061107.9229.4890.0550.0020.0040.0030.0770.0030.0020.0740.0030.0020.067106.5477.8430.0600.0020.0040.0030.0820.0030.0030.0810.0030.0030.073125.5626.530.0650.0020.00

10、40.0030.0870.0030.0030.0850.0030.0030.078134.7395.5640.0700.0020.0040.0030.0920.0030.0030.0910.0030.0030.083134.0864.7970.0750.0020.0040.0030.1000.0030.0030.0950.0030.0030.090143.70214.11900.0800.0030.0050.0040.1080.0030.0030.1030.0030.0030.095143.4253.4780.0850.0030.0050.0040.1130.0030.0030.1080.00

11、30.0030.100152.77853.2530.0900.0030.0050.0040.1180.0030.0030.1130.0030.0030.105152.4952.90.0950.0030.0050.0040.1230.0030.0030.1180.0030.0030.111152.4322.4630.1000.0030.0050.0040.1280.0030.0040.1250.0030.0040.116162.0342.3330.1100.0030.0050.0040.1380.0030.0040.1350.0030.0040.127171.71641.9170.1200.00

12、30.0060.0040.1520.0040.0040.1470.0030.0040.139171.4261.6040.1300.0030.0060.0040.1620.0040.0040.1570.0030.0040.150181.2201.3610.1400.0030.0060.0040.1720.0040.0040.1670.0030.0040.160181.0551.170.1500.0030.0060.0040.1820.0040.0040.1770.0030.0040.170190.92171.0160.1600.0030.0070.0040.1940.0050.0040.1890

13、.0050.0040.181190.81220.89060.1700.0030.0070.0040.2040.0050.0040.1990.0050.0040.191200.72100.78710.1800.0030.0080.0040.2160.0050.0050.2110.0050.0050.202200.64440.70070.1900.0030.0080.0040.2280.0050.0050.2210.0050.0050.212210.57930.62780.2000.0030.0080.0040.2380.0050.0050.2310.0050.0050.222210.52240.

14、56570.2100.0030.0080.0040.2480.0050.0050.2410.0050.0050.232210.47570.51230.2200.0040.0080.0040.2580.0050.0050.2520.0050.0050.242210.43400.46620.2300.0040.0090.0050.2720.0060.0050.2640.0060.0050.255220.39410.42980.2400.0040.0090.0050.2820.0060.0050.2740.0060.0050.265220.36250.39410.2500.0040.0090.005

15、0.2920.0060.0050.2840.0060.0050.275220.33450.36280.2600.0040.0090.0050.3050.0060.0050.2940.0060.0050.285220.30960.33500.2700.0040.0090.0050.3150.0060.0050.3040.0060.0050.295220.28740.31020.2800.0040.0090.0050.3250.0060.0050.3140.0060.0050.307220.26760.28820.2900.0040.0090.0050.3350.0060.0050.3240.00

16、60.0050.317220.24970.26840.3000.0050.0100.0060.3490.0070.0060.3370.0070.0060.328230.23350.25050.3100.0050.0100.0060.3590.0070.0060.3470.0070.0060.338230.21890.23440.3200.0050.0100.006.03690.0070.0060.3570.0070.0060.348230.20560.21980.3300.0050.0100.0060.3790.0070.0060.3670.0070.0060.358230.19340.206

17、10.3400.0050.0100.0060.3890.0070.0060.3770.0070.0060.368230.18240.19400.3500.0050.0100.0060.3990.0070.0060.3870.0070.0060.378230.17220.18300.3600.0050.0100.0060.4100.0070.0060.3970.0070.0060.388230.16200.17400.3700.0050.0100.0070.4200.0070.0060.4070.0070.0060.398240.15350.16480.3800.0050.0100.0070.4

18、300.0070.0060.4170.0070.0060.410240.14560.15610.3900.0050.0100.0070.4400.0070.0060.4270.0070.0060.421240.13830.14810.4000.0050.0110.0070.4500.0070.0060.4390.0070.0060.433240.13600.14070.4100.0050.0110.0070.4600.0070.0060.4490.0070.0060.443250.12530.13380.4200.0050.0110.0070.4700.0070.0060.4600.0070.

19、0060.453250.11950.12350.4300.0050.0110.0070.4800.0070.0060.4700.0070.0060.463250.11400.12150.4400.0050.0110.0070.4900.0070.0060.4800.0070.0060.473250.10900.11600.4500.0050.0110.0070.5020.0070.0060.4900.0070.0060.483250.10420.11090.4600.0050.0110.0070.5120.0070.0060.5000.0070.0060.493250.09980.10600.

20、4700.0050.0110.0070.5220.0070.0060.5120.0070.0060.504250.09570.10150.4800.0050.0110.0070.5340.0070.0060.5220.0070.0060.515250.09170.09730.4900.0050.0110.0070.5440.0070.0060.5320.0070.0060.526250.08810.09330.5000.0050.0120.0070.5560.0080.0060.5420.0080.0060.537250.08460.08900.5100.0060.0120.0070.5660

21、.0080.0060.5520.0080.0060.548260.081050.086420.5200.0060.0120.0070.5780.0080.0060.5640.0080.0060.558260.078000.083090.5300.0060.0120.0070.5880.0080.0060.5760.0080.0060.569260.075110.079950.5400.0060.0120.0070.6980.0080.0060.5880.0080.0060.579260.072390.076980.5500.0060.0130.0080.6100.0090.0070.6000.

22、0090.0070.59260.069810.074180.5700.0060.0130.0080.6300.0090.0070.6200.0090.0070.61260.065040.069010.5800.0060.0130.0080.6400.0090.0070.6300.0090.0070.62260.062840.066630.5900.0060.0130.0080.6500.0090.0070.6400.0090.0070.63260.060750.064360.6000.0070.0130.0080.6600.0090.0070.6500.0090.0070.64260.0587

23、60.062224.6、回彈性標(biāo)稱直徑0.0801.000mm的漆包線的回彈角應(yīng)符合表3規(guī)定。表3導(dǎo)體標(biāo)準(zhǔn)直徑mm圓棒直徑mm負(fù)荷 N最大回彈角度導(dǎo)體標(biāo)準(zhǔn)直徑mm圓棒直徑mm負(fù)荷 N最大回彈角度1級(jí)2級(jí)3級(jí)1級(jí)2級(jí)3級(jí)0.08050.2510080700.400194.05550450.09050.259477670.450258.05348440.10050.259073640.500258.05147430.11270.508873640.560258.04844410.12570.508470620.63037.512.05350460.14070.507967590.71037.512

24、.05047440.160101.07867590.800. 37.512.04643410.180101.07565570.9005015.05148450.200101.07262541.0005015.04745420.22412.52.06859510.25012.52.06556490.28012.52.06153470.315194.06255500.355194.0595348注：介于相鄰標(biāo)稱直徑間的中間規(guī)格，取較大標(biāo)稱直徑相應(yīng)的回彈角值。4.7、熱沖擊按表4規(guī)定，卷繞或伸長(zhǎng)的試樣，在1505溫度下放置30min以后，用約15倍的放大鏡檢查漆膜應(yīng)不開裂。表4標(biāo)稱直徑 mm卷 繞伸

25、長(zhǎng) %試棒直徑 mmd0.04卷繞前伸長(zhǎng)20%或拉伸至斷裂點(diǎn)0.1500.040d0.160取較小值3d0.160d0.250取較小值4d0.250d0.600取較小值2d4.8、軟化擊穿在170溫度下，2min以內(nèi)不擊穿。4.9、擊穿電壓4.9.1、標(biāo)稱直徑0.100mm及以下的漆包線，用圓棒法試驗(yàn)，其擊穿電壓應(yīng)符合表5。表5標(biāo)稱直徑 dmm最小擊穿電壓 V（有效值）標(biāo)稱直徑 dmm最小擊穿電壓 V（有效值）0.0201200.0553250.0251500.063750.0281700.0654250.0301900.074250.0352250.084250.0382500.085500

26、0.0402500.0905000.0452750.0955000.053000.1005004.9.2、標(biāo)稱直徑0.1121.00mm的漆包線用扭絞法試驗(yàn)，其擊穿電壓應(yīng)符合表6。表6標(biāo)稱直徑 dmm最小擊穿電壓 V（有效值）標(biāo)稱直徑 dmm最小擊穿電壓 V0.1113000.2521000.1215000.2822000.1316000.31522000.1417000.35523000.1517000.40023000.1617000.45023000.1717000.50024000.1817000.53025000.1920000.56025000.2020000.6002600注：對(duì)

27、于中間規(guī)格，擊穿電壓值取最接近較大一檔規(guī)格的數(shù)值。4.10、常態(tài)針孔漆包線最大針孔數(shù)為10個(gè)。4.11、焊錫性漆包線試樣，浸入溫度為3755的焊錫槽中，不超過2S，即能完全潤(rùn)錫，搪錫線表面應(yīng)平滑，無針孔及漆膜殘?jiān)?.12、粘合強(qiáng)度4.12.1、不發(fā)粘性按表7規(guī)定扭絞，在605溫度下，保溫1小時(shí)試驗(yàn)應(yīng)不發(fā)粘。表7導(dǎo)體標(biāo)稱直徑（mm）負(fù)荷（N）125mm中的扭絞數(shù)0.050.0294500.060.070.049400.080.110.098300.120.170.392240.180.201.176200.210.241.47160.250.371.692120.400.601.96104.1

28、2.2、粘結(jié)強(qiáng)度按表8定的張力進(jìn)行卷繞，粘結(jié)力應(yīng)符合表9規(guī)定。表8標(biāo)稱直徑（mm）卷繞力（N）0.0250.0450.0490.0500.0800.1960.0900.1400.490.1500.2000.980.2100.2401.960.2500.3702.940.400.6004.904.13、耐溶劑漆包線在標(biāo)準(zhǔn)溶劑中浸泡過后，目測(cè)漆膜無溶脹現(xiàn)象，浸泡后漆膜的硬度應(yīng)不小于“H”。4.14、耐藥品性漆包線在規(guī)定的溶劑中處理后，絕緣漆膜無起泡和溶脹現(xiàn)象，用指尖刮或用鉛筆推時(shí)，絕緣漆膜不應(yīng)整片剝落。表9標(biāo)稱直徑（mm）平均粘接力（N）0.040.050.1450.060.070.1960.08

29、0.2450.0850.2940.090.3430.100.110.3920.120.140.4410.150.170.490.180.190.5880.200.210.6860.220.7350.230.290.7840.300.400.8860.410.600.9805、 試驗(yàn)方法5.1、試驗(yàn)環(huán)境a、試驗(yàn)應(yīng)在溫度為15-35，相對(duì)濕度為45%-75%的環(huán)境條件下進(jìn)行。b、試驗(yàn)前，試樣必須在上述環(huán)境條件下放置8小時(shí)以上，使試樣獲得穩(wěn)定狀態(tài)。5.2、取樣規(guī)則試樣應(yīng)從整軸的漆包線上選取。取樣時(shí)漆包線不得受到拉伸和過分彎曲，每次取樣前，應(yīng)從線軸上去掉足夠的漆包線，以保證取樣中不夾帶任何損壞的線段。

30、5.3表面質(zhì)量對(duì)成軸漆包線的表面質(zhì)量，用肉眼觀察、手摸、指甲摩刮等方法進(jìn)行以下項(xiàng)目的檢查。a、有無外傷、沾污；b、表面光滑、光澤與顏色的均勻性；c、是否發(fā)粘；d、用指甲摩刮，漆膜是否容易剝落。5.4、常態(tài)針孔導(dǎo)體直徑0.06mm以下取長(zhǎng)約1.5m，導(dǎo)體直徑0.07mm以上，取長(zhǎng)約6m試樣，浸入0.2%的食鹽水中在食鹽水里滴有適量的3%酒精酚酞溶液，試樣浸入長(zhǎng)度為5m，溶液按正極，試驗(yàn)接負(fù)極，施以12V直流電壓1分鐘后，檢查產(chǎn)生的針孔數(shù)。5.5、粘結(jié)強(qiáng)度試驗(yàn)5.5.1、不發(fā)粘性導(dǎo)體直徑為0.05mm及以上的漆包線，取長(zhǎng)約50cm的試樣，按表7規(guī)定扭絞，然后在605的恒溫箱中保溫1小時(shí)取出，當(dāng)試樣

31、的溫度降至室溫時(shí)，將扭絞對(duì)反扭絞，檢查試樣是否發(fā)粘。5.5.2、粘結(jié)力試驗(yàn)按表8規(guī)定的張力，用旋轉(zhuǎn)軸型卷繞機(jī)把被測(cè)試樣線在19.5mm經(jīng)醇溶性自粘漆浸漬過的紙管上密繞2050圈，繞二層作為試樣，但在做溶劑粘結(jié)試驗(yàn)時(shí)，應(yīng)當(dāng)是邊通過溶劑槽，邊卷繞。通過溶劑槽邊卷繞而制得的試樣，在室溫下放置20分鐘，然后在1005的恒溫箱中干燥處理10分鐘后粘接。試樣冷卻至室溫后，測(cè)定粘接的線與線之間的重量，粘結(jié)力用最大值和最小值的平均值表示。5.6、耐藥品性試驗(yàn)試樣為2個(gè)，1個(gè)使用試劑（1），另一個(gè)使用試劑（2）。（1） 用蒸餾水或者去離子水配置的比重為1.20的硫酸溶液用來配置的，硫酸應(yīng)為試劑；（2） 用蒸餾水或去離子水配置的濃度為10%的氫氧化鈉水溶液，用來配置的氫氧化鈉應(yīng)為溶劑。取長(zhǎng)約20cm的試樣，在1255的恒溫箱中加熱處理10分鐘，試樣應(yīng)不受彎曲和拉伸，將試樣浸入10-30的上述溶液中，浸入長(zhǎng)